N-Methyl-2-aminopyridine-3-carboxamide

Product Name: N-Methyl-2-aminopyridine-3-carboxamide
CAS No.: 870997-87-8
Chemical Name: N-Methyl-2-aminopyridine-3-carboxamide
Synonyms: N-Methyl-2-aminonicotinamide;2-Amino-N-methylnicotinamide;N-methyl-2-amino-3-nicotinamide;2-amino-N-methylpyridine-3-carboxamide;N-Methyl-2-aminopyridine-3-carboxamide;3-Pyridinecarboxamide,2-amino-N-methyl-;N-Methyl-2-aminopyridine-3-carboxamide ISO 9001：2015 REACH
CBNumber: CB02462174
Molecular Formula: C7H9N3O
Formula Weight: 151.17
MOL File: 870997-87-8.mol

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N-Methyl-2-aminopyridine-3-carboxamide Property

Melting point:: 149 - 151°C
Boiling point:: 373.1±27.0 °C(Predicted)
Density: 1.206
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
solubility: DMSO (Slightly), Methanol (Slightly, Sonicated)
form: Solid
pka: 14.44±0.46(Predicted)
color: White to Off-White

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H312Harmful in contact with skin

H332Harmful if inhaled

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: A636380
Product name: 2-Amino-N-methylpyridine-3-carboxamide
Packaging: 250mg
Price: $75
Updated: 2021/12/16

TRC

Product number: A636380
Product name: 2-Amino-N-methylpyridine-3-carboxamide
Packaging: 500mg
Price: $120
Updated: 2021/12/16

AK Scientific

Product number: 3745AC
Product name: 2-Amino-N-methylnicotinamide
Packaging: 100mg
Price: $73
Updated: 2021/12/16

AK Scientific

Product number: 3745AC
Product name: 2-Amino-N-methylnicotinamide
Packaging: 250mg
Price: $85
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0079763
Product name: N-METHYL-2-AMINONICOTINAMIDE
Purity: 95.00%
Packaging: 5G
Price: $909.56
Updated: 2021/12/16

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N-Methyl-2-aminopyridine-3-carboxamide Chemical Properties,Usage,Production

Uses

2-Amino-N-methylpyridine-3-carboxamide is used in preparation of triazolopyrazine derivatives and analogs for use as c-MET kinase activity inhibitors.

Synthesis

5345-47-1

593-51-1

870997-87-8

To 2-aminonicotinic acid (2.0 g, 14.5 mmol) and methylamine hydrochloride (1.47 g, 1.5 eq.) were added EDC (4.49 g, 1.5 eq.), HOBt (2.35 g, 1.2 eq.), and DIEA (7.6 mL, 3.0 eq.) sequentially in DMF (20 mL). The reaction mixture was stirred at room temperature overnight. Upon completion of the reaction, the crude product was concentrated and the residue was dissolved in EtOAc. The organic phase was washed with saturated NaHCO3 solution. After removing the solvent under reduced pressure, the crude product was purified by silica gel column chromatography (eluent: 0%-20% MeOH/DCM) to afford the target compound 2-amino-N-methylnicotinamide (2.16 g, isolated yield 98%).

References

[1] Patent: WO2008/115369, 2008, A2. Location in patent: Page/Page column 130

N-Methyl-2-aminopyridine-3-carboxamide Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from N-Methyl-2-aminopyridine-3-carboxamide manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: N-Methyl-2-aminopyridine-3-carboxamide 870997-87-8
Price: US $1.10/g
Min. Order: 1g
Purity: 99.0% min
Supply Ability: 100 tons min
Release date: 2021-05-07

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N-Methyl-2-aminopyridine-3-carboxamide ISO 9001：2015 REACH

870997-87-8