N-METHOXY-N-METHYLCYCLOPROPANECARBOXAMIDE
- Product Name
- N-METHOXY-N-METHYLCYCLOPROPANECARBOXAMIDE
- CAS No.
- 147356-78-3
- Chemical Name
- N-METHOXY-N-METHYLCYCLOPROPANECARBOXAMIDE
- Synonyms
- opropanecarboxamide;N-METHOXY-N-METHYL-CYCLOPROPANAMIDE;N-METHOXY-N-METHYLCYCLOPROPANECARBOXAMIDE;Cyclopropanecarboxamide, N-methoxy-N-methyl-;cyclopropanecarboxylic acid N-methoxy-N-methylamide;N-methoxy-N-methylcyclopropanecarboxamide(WXC04265)
- CBNumber
- CB02464820
- Molecular Formula
- C6H11NO2
- Formula Weight
- 129.16
- MOL File
- 147356-78-3.mol
N-METHOXY-N-METHYLCYCLOPROPANECARBOXAMIDE Property
- Boiling point:
- 151.5±23.0 °C(Predicted)
- Density
- 1.126±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C
- Appearance
- Colorless to light yellow Liquid
Safety
- Safety Statements
- 24/25
- HS Code
- 29241990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
N-Bromosuccinimide Price
- Product number
- M271788
- Product name
- N-Methoxy-N-methylcyclopropanecarboxamide
- Packaging
- 250mg
- Price
- $55
- Updated
- 2021/12/16
- Product number
- 459311
- Product name
- N-Methoxy-N-methylcyclopropanecarboxamide
- Packaging
- 100mg
- Price
- $305
- Updated
- 2021/12/16
- Product number
- J93810
- Product name
- N-Methoxy-N-methylcyclopropanecarboxamide
- Packaging
- 1g
- Price
- $25
- Updated
- 2021/12/16
- Product number
- 4256-1-24
- Product name
- N-Methoxy-N-methylcyclopropanecarboxamide
- Packaging
- 1g
- Price
- $474
- Updated
- 2021/12/16
- Product number
- J93810
- Product name
- N-Methoxy-N-methylcyclopropanecarboxamide
- Packaging
- 100g
- Price
- $750
- Updated
- 2021/12/16
N-METHOXY-N-METHYLCYCLOPROPANECARBOXAMIDE Chemical Properties,Usage,Production
Synthesis
6638-79-5
4023-34-1
147356-78-3
To a solution of dichloromethane (60 mL) containing N,O-dimethylhydroxylamine hydrochloride (10.0 g, 95.69 mmol, 1.0 eq.) and triethylamine (19.36 g, 191.6 mmol, 2.0 eq.), the reaction mixture was stirred at 0 °C for 30 min. Subsequently, cyclopropanecarbonyl chloride (Compound 96.1) was slowly added at the same temperature. The reaction mixture was transferred to room temperature and continued stirring for 15 hours. After completion of the reaction, the organic layer was washed sequentially with water, brine, saturated sodium bicarbonate solution and 1.0 N hydrochloric acid, dried over anhydrous sodium sulfate and concentrated under reduced pressure to give the crude product. Finally, the crude product was purified by column chromatography to afford N-methoxy-N-methylcyclopropane carboxamide (Compound 96.2, 9.0 g, 72.9% yield).
References
[1] Journal of Medicinal Chemistry, 2017, vol. 60, # 12, p. 4840 - 4860
[2] Patent: WO2017/40757, 2017, A1. Location in patent: Paragraph 00466-00467
[3] Patent: US2005/197337, 2005, A1. Location in patent: Page/Page column 10
[4] Patent: WO2005/94828, 2005, A1. Location in patent: Page/Page column 19
[5] Patent: WO2008/34860, 2008, A1. Location in patent: Page/Page column 139
N-METHOXY-N-METHYLCYCLOPROPANECARBOXAMIDE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from N-METHOXY-N-METHYLCYCLOPROPANECARBOXAMIDE manufacturers
- Product
- N-METHOXY-N-METHYLCYCLOPROPANECARBOXAMIDE 147356-78-3
- Price
- US $1.00/kg
- Min. Order
- 1kg
- Purity
- 95%-99%
- Supply Ability
- 100kg
- Release date
- 2018-12-22