2-ForMylisonicotinic acid
- Product Name
- 2-ForMylisonicotinic acid
- CAS No.
- 855636-38-3
- Chemical Name
- 2-ForMylisonicotinic acid
- Synonyms
- 2-ForMylisonicotinic acid;2-formyl-4-Pyridinecarboxylic acid;2-formylpyridine-4-carboxylic acid;4-Pyridinecarboxylic acid, 2-formyl-
- CBNumber
- CB02727538
- Molecular Formula
- C7H5NO3
- Formula Weight
- 151.12
- MOL File
- 855636-38-3.mol
2-ForMylisonicotinic acid Property
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- F754670
- Product name
- 2-FormylisonicotinicAcid
- Packaging
- 25mg
- Price
- $155
- Updated
- 2021/12/16
- Product number
- 3286AC
- Product name
- 2-Formylisonicotinicacid
- Packaging
- 1g
- Price
- $3117
- Updated
- 2021/12/16
- Product number
- CD11044191
- Product name
- 2-Formylisonicotinicacid
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $251
- Updated
- 2021/12/16
- Product number
- CM178861
- Product name
- 2-formylisonicotinicacid
- Purity
- 95%
- Packaging
- 1g
- Price
- $511
- Updated
- 2021/12/16
- Product number
- CD11044191
- Product name
- 2-Formylisonicotinicacid
- Purity
- 95+%
- Packaging
- 1g
- Price
- $875
- Updated
- 2021/12/16
2-ForMylisonicotinic acid Chemical Properties,Usage,Production
Synthesis
4021-11-8
855636-38-3
2-Methyl-4-pyridinecarboxylic acid (5.0 g, 36.5 mmol) was used as raw material and mixed with selenium dioxide (10.1 g, 91.3 mmol) in 250 ml of dioxane. The reaction mixture was heated to 110°C and the reaction was continued under magnetic stirring for 24 hours. The reaction process was monitored by thin layer chromatography (TLC). Upon completion of the reaction, the reaction mixture was filtered while hot to remove insoluble impurities. Subsequently, the solvent was removed by distillation under reduced pressure to obtain the crude product. The crude product was purified by recrystallization from anhydrous ethanol and finally dried under vacuum to give 2-formyl-4-pyridinecarboxylic acid as a white solid in 72% yield and 98% purity.
References
[1] Patent: CN107686464, 2018, A. Location in patent: Paragraph 0021; 0022; 0024; 0026; 0028; 0030
2-ForMylisonicotinic acid Preparation Products And Raw materials
Raw materials
Preparation Products
2-ForMylisonicotinic acid Suppliers
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