Dodecanoic acid, 12-bromo-, ethyl ester

Product Name: Dodecanoic acid, 12-bromo-, ethyl ester
CAS No.: 72338-48-8
Chemical Name: Dodecanoic acid, 12-bromo-, ethyl ester
Synonyms: ETHYL 12-BROMODODECANOATE;12-Bromododecanoic acid ethyl ester;Dodecanoic acid, 12-bromo-, ethyl ester
CBNumber: CB02756202
Molecular Formula: C14H27BrO2
Formula Weight: 307.27
MOL File: 72338-48-8.mol

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Dodecanoic acid, 12-bromo-, ethyl ester Property

Boiling point:: 338.7±15.0 °C(Predicted)
Density: 1.112±0.06 g/cm3(Predicted)
storage temp.: Store at room temperature
Appearance: Colorless to light yellow Liquid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

Ambeed

Product number: A121528
Product name: Ethyl12-bromododecanoate
Purity: 97%
Packaging: 100mg
Price: $19
Updated: 2021/12/16

Ambeed

Product number: A121528
Product name: Ethyl12-bromododecanoate
Purity: 97%
Packaging: 250mg
Price: $30
Updated: 2021/12/16

Ambeed

Product number: A121528
Product name: Ethyl12-bromododecanoate
Purity: 97%
Packaging: 1g
Price: $73
Updated: 2021/12/16

Ambeed

Product number: A121528
Product name: Ethyl12-bromododecanoate
Purity: 97%
Packaging: 5g
Price: $251
Updated: 2021/12/16

Crysdot

Product number: CD13005709
Product name: Ethyl12-bromododecanoate
Purity: 97%
Packaging: 5g
Price: $495
Updated: 2021/12/16

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Dodecanoic acid, 12-bromo-, ethyl ester Chemical Properties,Usage,Production

Synthesis

78640-13-8

72338-48-8

b) Synthesis of ethyl 12-bromododecanoate Ethyl 12-hydroxydodecanoate (1.65 g, 6.7 mmol) was dissolved in dichloromethane (20 mL) under nitrogen protection in a 100 mL two-necked round-bottomed flask equipped with a reflux condenser tube and a magnetic stirrer. Triphenylphosphine (PPh3, 1.93 g, 7.4 mmol) and N-bromosuccinimide (NBS, 1.6 g, 7.0 mmol) were added sequentially. The reaction mixture was stirred under reflux conditions for 24 hours. Upon completion of the reaction, the reaction solution was concentrated using a rotary evaporator and the resulting crude product was purified by silica gel column chromatography with petroleum ether/ethyl acetate (5:1, v/v) as eluent. The final isolation afforded 1.92 g of ethyl 12-bromododecanoate in 92% yield as a light yellow oil.

References

[1] Patent: EP1979365, 2012, B1. Location in patent: Page/Page column 9
[2] Patent: US8816107, 2014, B2. Location in patent: Page/Page column 11
[3] Journal of the American Chemical Society, 2003, vol. 125, # 14, p. 4174 - 4184

Dodecanoic acid, 12-bromo-, ethyl ester Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from Dodecanoic acid, 12-bromo-, ethyl ester manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD

Product: ethyl 12-bromododecanoate 72338-48-8
Price: US $2.20-8.80/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 50kg
Release date: 2025-06-24

PNP Biotech Co. Ltd

Product: Dodecanoic acid, 12-bromo-, ethyl ester 72338-48-8
Price: US $0.00/kg
Min. Order: 25kg
Purity: 95%
Supply Ability: Inquiry
Release date: 2022-09-28

72338-48-8, Dodecanoic acid, 12-bromo-, ethyl esterRelated Search:

ETHYL 12-BROMODODECANOATE

Dodecanoic acid, 12-bromo-, ethyl ester

12-Bromododecanoic acid ethyl ester

72338-48-8