Dodecanoic acid, 12-bromo-, ethyl ester
- Product Name
- Dodecanoic acid, 12-bromo-, ethyl ester
- CAS No.
- 72338-48-8
- Chemical Name
- Dodecanoic acid, 12-bromo-, ethyl ester
- Synonyms
- ETHYL 12-BROMODODECANOATE;12-Bromododecanoic acid ethyl ester;Dodecanoic acid, 12-bromo-, ethyl ester
- CBNumber
- CB02756202
- Molecular Formula
- C14H27BrO2
- Formula Weight
- 307.27
- MOL File
- 72338-48-8.mol
Dodecanoic acid, 12-bromo-, ethyl ester Property
- Boiling point:
- 338.7±15.0 °C(Predicted)
- Density
- 1.112±0.06 g/cm3(Predicted)
- storage temp.
- Store at room temperature
- Appearance
- Colorless to light yellow Liquid
N-Bromosuccinimide Price
- Product number
- A121528
- Product name
- Ethyl12-bromododecanoate
- Purity
- 97%
- Packaging
- 100mg
- Price
- $19
- Updated
- 2021/12/16
- Product number
- A121528
- Product name
- Ethyl12-bromododecanoate
- Purity
- 97%
- Packaging
- 250mg
- Price
- $30
- Updated
- 2021/12/16
- Product number
- A121528
- Product name
- Ethyl12-bromododecanoate
- Purity
- 97%
- Packaging
- 1g
- Price
- $73
- Updated
- 2021/12/16
- Product number
- A121528
- Product name
- Ethyl12-bromododecanoate
- Purity
- 97%
- Packaging
- 5g
- Price
- $251
- Updated
- 2021/12/16
- Product number
- CD13005709
- Product name
- Ethyl12-bromododecanoate
- Purity
- 97%
- Packaging
- 5g
- Price
- $495
- Updated
- 2021/12/16
Dodecanoic acid, 12-bromo-, ethyl ester Chemical Properties,Usage,Production
Synthesis
78640-13-8
72338-48-8
b) Synthesis of ethyl 12-bromododecanoate Ethyl 12-hydroxydodecanoate (1.65 g, 6.7 mmol) was dissolved in dichloromethane (20 mL) under nitrogen protection in a 100 mL two-necked round-bottomed flask equipped with a reflux condenser tube and a magnetic stirrer. Triphenylphosphine (PPh3, 1.93 g, 7.4 mmol) and N-bromosuccinimide (NBS, 1.6 g, 7.0 mmol) were added sequentially. The reaction mixture was stirred under reflux conditions for 24 hours. Upon completion of the reaction, the reaction solution was concentrated using a rotary evaporator and the resulting crude product was purified by silica gel column chromatography with petroleum ether/ethyl acetate (5:1, v/v) as eluent. The final isolation afforded 1.92 g of ethyl 12-bromododecanoate in 92% yield as a light yellow oil.
References
[1] Patent: EP1979365, 2012, B1. Location in patent: Page/Page column 9
[2] Patent: US8816107, 2014, B2. Location in patent: Page/Page column 11
[3] Journal of the American Chemical Society, 2003, vol. 125, # 14, p. 4174 - 4184
Dodecanoic acid, 12-bromo-, ethyl ester Preparation Products And Raw materials
Raw materials
Preparation Products
Dodecanoic acid, 12-bromo-, ethyl ester Suppliers
- Tel
- --
- Fax
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- info@synthonix.com
- Country
- United States
- ProdList
- 6872
- Advantage
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View Lastest Price from Dodecanoic acid, 12-bromo-, ethyl ester manufacturers
- Product
- ethyl 12-bromododecanoate 72338-48-8
- Price
- US $2.20-8.80/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 50kg
- Release date
- 2025-06-24
- Product
- Dodecanoic acid, 12-bromo-, ethyl ester 72338-48-8
- Price
- US $0.00/kg
- Min. Order
- 25kg
- Purity
- 95%
- Supply Ability
- Inquiry
- Release date
- 2022-09-28