3,5-DICHLORO-4-HYDROXYBENZALDEHYDE

Product Name: 3,5-DICHLORO-4-HYDROXYBENZALDEHYDE
CAS No.: 2314-36-5
Chemical Name: 3,5-DICHLORO-4-HYDROXYBENZALDEHYDE
Synonyms: NSC 31590;AKOS B029235;Nipaguard DCHB 30;2,6-Dichloro-4-formylphenol;5-DICHLORO-4-HYDROXYBENZALDEHYDE;3,5-Dichloro-4-hydroxybenzaldehyd;3,5-DICHLORO-4-HYDROXYBENZALDEHYDE;Benzaldehyde, 3,5-dichloro-4-hydroxy-
CBNumber: CB0331629
Molecular Formula: C7H4Cl2O2
Formula Weight: 191.01
MOL File: 2314-36-5.mol

More

Less

3,5-DICHLORO-4-HYDROXYBENZALDEHYDE Property

Melting point:: 154 °C
Boiling point:: 256.7±35.0 °C(Predicted)
Density: 1.547±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
form: solid
pka: 4.85±0.23(Predicted)
color: White
InChI: 1S/C7H4Cl2O2/c8-5-1-4(3-10)2-6(9)7(5)11/h1-3,11H
InChIKey: LIYGCLJYTHRBQV-UHFFFAOYSA-N
SMILES: Oc1c(Cl)cc(C=O)cc1Cl
CAS DataBase Reference: 2314-36-5

More

Less

Safety

Hazard Codes: Xi
Risk Statements: 36
Safety Statements: 26
WGK Germany: WGK 3
Hazard Note: Irritant
HS Code: 2913000090
Storage Class: 11 - Combustible Solids
Hazard Classifications: Eye Irrit. 2
Skin Irrit. 2
STOT SE 3

More

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More

Less

N-Bromosuccinimide Price

TRC

Product number: D438693
Product name: 3,5-Dichloro-4-hydroxybenzaldehyde
Packaging: 100mg
Price: $60
Updated: 2021/12/16

TRC

Product number: D438693
Product name: 3,5-Dichloro-4-hydroxybenzaldehyde
Packaging: 500mg
Price: $90
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD70957
Product name: 3,5-Dichloro-4-hydroxybenzaldehyde
Packaging: 5G
Price: $125
Updated: 2021/12/16

Apolloscientific

Product number: OR27469
Product name: 3,5-Dichloro-4-hydroxybenzaldehyde
Packaging: 5g
Price: $128
Updated: 2021/12/16

Matrix Scientific

Product number: 076585
Product name: 3,5-Dichloro-4-hydroxybenzaldehyde
Purity: 95+%
Packaging: 5g
Price: $138
Updated: 2021/12/16

More

Less

3,5-DICHLORO-4-HYDROXYBENZALDEHYDE Chemical Properties,Usage,Production

Uses

3,5-Dichloro-4-hydroxybenzaldehyde (cas# 2314-36-5) is a useful research chemical. It is used in fluorescent dye, preparation method therefor and use thereof.

Synthesis

2432-12-4

2314-36-5

General procedure for the synthesis of 3,5-dichloro-4-hydroxybenzaldehyde from 2,6-dichloro-4-methylphenol: A mixture of the substrate 2,6-dichloro-4-methylphenol (1 mmol), cobalt salts (n1 mol%), and NaOH (n2 equiv.) in ethylene glycol (5 mL) was subjected to a stirring reaction under an atmosphere of oxygen (1 atm) at 80°C for 8 hours. Upon completion of the reaction, hydrochloric acid (10 mL, 2%) and methyl tert-butyl ether (MTBE, 10 mL) were sequentially added to the reaction mixture. The organic layer was separated and the aqueous phase was further extracted with MTBE (10 mL x 2). All organic phases were combined, dried with anhydrous sodium sulfate and concentrated to obtain the residue. The residue was purified by silica gel column chromatography (eluent: petroleum ether/ethyl acetate, 10:1, v/v) to afford the target product 3,5-dichloro-4-hydroxybenzaldehyde.

References

[1] Tetrahedron Letters, 2014, vol. 55, # 8, p. 1406 - 1411
[2] Green Chemistry, 2014, vol. 16, # 5, p. 2807 - 2814
[3] Green Chemistry, 2014, vol. 16, # 3, p. 1248 - 1254

3,5-DICHLORO-4-HYDROXYBENZALDEHYDE Preparation Products And Raw materials

Raw materials

Preparation Products

More

Less

3,5-DICHLORO-4-HYDROXYBENZALDEHYDE Suppliers

Belgium 1 China 97 Germany 1 India 1 Russia 1 Slovakia 1 Switzerland 2 The Netherlands 1 United Kingdom 9 United States 15 Global 129

J & K SCIENTIFIC LTD.

Tel: 18210857532; 18210857532
Fax: 86-10-82849933
Email: jkinfo@jkchemical.com
Country: China
ProdList: 96815
Advantage: 76

Energy Chemical

Tel: 021-021-58432009 400-005-6266
Fax: 021-58436166
Email: sales8178@energy-chemical.com
Country: China
ProdList: 44801
Advantage: 61

Shanghai Harvest Chemical Industrial Co., Ltd.

Tel: 021-31038972,31038973 17321035817
Fax: +86-21-51385350
Email: sales@harvest-chem.com
Country: China
ProdList: 2818
Advantage: 64

Shanghai Hanhong Scientific Co.,Ltd.

Tel: 021-54306202 13764082696
Email: info@hanhongsci.com
Country: China
ProdList: 42934
Advantage: 64

Shanghai Sunway Pharmaceutical Technology Co., Ltd

Tel: 18270980682
Fax: 021 51613951
Email: mlcheng@sunwaypharm.cn
Country: China
ProdList: 8667
Advantage: 57

T&W GROUP

Tel: 021-61551611 13296011611
Fax: ＋86 21-50676805
Email: contact@trustwe.com
Country: China
ProdList: 9895
Advantage: 58

Thermo Fisher Scientific

Tel: 800-810-5118
Fax: +86-10-84193589
Email: cnchemical@thermofisher.com
Country: China
ProdList: 17770
Advantage: 75

Shanghai Topbiochem Technology Co., Ltd

Tel: +86-21-60341587
Fax: +86-21-61294319
Email: sales@topbiochem.com
Country: China
ProdList: 6175
Advantage: 58

Nanjing Norris-Pharm Technology Co., Ltd

Tel: 18652989687
Fax: +86-25-52131256
Email: sales@norris-pharm.com
Country: China
ProdList: 8878
Advantage: 55

9ding chemical ( Shanghai) Limited

Tel: 4009209199
Fax: 86-021-52271987
Email: sales@9dingchem.com
Country: China
ProdList: 22514
Advantage: 55

More

Less

View Lastest Price from 3,5-DICHLORO-4-HYDROXYBENZALDEHYDE manufacturers

Career Henan Chemical Co

Product: 3,5-DICHLORO-4-HYDROXYBENZALDEHYDE 2314-36-5
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100kg
Release date: 2019-07-12

2314-36-5, 3,5-DICHLORO-4-HYDROXYBENZALDEHYDERelated Search:

METHYL 3,5-DICHLORO-4-HYDROXYBENZOATE ETHYL 3,5-DICHLORO-4-HYDROXYBENZOATE 3,5-Dichloro-4-hydroxybenzoic acid 3,5-DICHLORO-4-PROPOXYBENZOIC ACID 2,3-Dichloro-4-hydroxybenzaldehyde 97%,2,3-DICHLORO-4-HYDROXYBENZALDEHYDE 3,5-DICHLORO-2-HYDROXYBENZALDEHYDE 4,6-DICHLORO-2-HYDROXYBENZALDEHYDE,2,4-DICHLORO-6-HYDROXYBENZALDEHYDE 3,5-DICHLORO-4-METHOXYBENZOIC ACID 3,5-DICHLORO-4-METHOXYBENZOIC ACID ETHYL ESTER 3,5-DICHLORO-4-HYDROXYBENZOIC ACID PROPYL ESTER 3,5-DICHLORO-4-HYDROXYBENZOHYDRAZIDE avilamycin A 1-((3,5-dichloro)-2,6-dihydroxy-4-methoxyphenyl)-1-hexanone METHYL 3,5-DICHLORO-4-METHOXYBENZOATE 3',5'-DICHLORO-4'-HYDROXYACETOPHENONE 4-(BENZYLOXY)-3,5-DICHLOROBENZALDEHYDE 3,5-DICHLORO-4-METHOXYBENZENECARBOHYDRAZIDE 4-(Allyloxy)-3,5-dichlorobenzoic acid

3,5-DICHLORO-4-HYDROXYBENZALDEHYDE

AKOS B029235

Benzaldehyde, 3,5-dichloro-4-hydroxy-

2,6-Dichloro-4-formylphenol

Nipaguard DCHB 30

NSC 31590

5-DICHLORO-4-HYDROXYBENZALDEHYDE

3,5-Dichloro-4-hydroxybenzaldehyd

2314-36-5

ALDEHYDE

Aromatic Aldehydes & Derivatives (substituted)

Aldehydes

Phenyls & Phenyl-Het