1-(4-Hydroxy-3,5-dimethoxyphenyl)-2-(2-methoxyphenoxy)propane-1,3-diol

Product Name: 1-(4-Hydroxy-3,5-dimethoxyphenyl)-2-(2-methoxyphenoxy)propane-1,3-diol
CAS No.: 92409-34-2
Chemical Name: 1-(4-Hydroxy-3,5-dimethoxyphenyl)-2-(2-methoxyphenoxy)propane-1,3-diol
Synonyms: 1-(4-Hydroxy-3,5-dimethoxyphenyl)-2-(2-methoxyphenoxy)propane-1,3-diol;1,3-Propanediol,1-(4-hydroxy-3,5-dimethoxyphenyl)-2-(2-methoxyphenoxy)-
CBNumber: CB13052470
Molecular Formula: C18H22O7
Formula Weight: 350.36
MOL File: 92409-34-2.mol

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1-(4-Hydroxy-3,5-dimethoxyphenyl)-2-(2-methoxyphenoxy)propane-1,3-diol Property

Boiling point:: 581.1±50.0 °C(Predicted)
Density: 1.279±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 9.93±0.36(Predicted)
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

AK Scientific

Product number: 8285CU
Product name: 1-(4-Hydroxy-3,5-dimethoxyphenyl)-2-(2-methoxyphenoxy)propane-1,3-diol
Packaging: 1g
Price: $1362
Updated: 2021/12/16

Ambeed

Product number: A176942
Product name: 1-(4-Hydroxy-3,5-dimethoxyphenyl)-2-(2-methoxyphenoxy)propane-1,3-diol
Purity: 96%
Packaging: 100mg
Price: $232
Updated: 2021/12/16

Crysdot

Product number: CD12006398
Product name: 1-(4-Hydroxy-3,5-dimethoxyphenyl)-2-(2-methoxyphenoxy)propane-1,3-diol
Purity: 96%
Packaging: 100mg
Price: $243
Updated: 2021/12/16

Alichem

Product number: 92409342
Product name: 1-(4-Hydroxy-3,5-dimethoxyphenyl)-2-(2-methoxyphenoxy)propane-1,3-diol
Packaging: 100mg
Price: $249.9
Updated: 2021/12/16

Ambeed

Product number: A176942
Product name: 1-(4-Hydroxy-3,5-dimethoxyphenyl)-2-(2-methoxyphenoxy)propane-1,3-diol
Purity: 96%
Packaging: 250mg
Price: $367
Updated: 2021/12/16

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1-(4-Hydroxy-3,5-dimethoxyphenyl)-2-(2-methoxyphenoxy)propane-1,3-diol Chemical Properties,Usage,Production

Synthesis

535967-76-1

92409-34-2

1-(4-(Benzyloxy)-3,5-dimethoxyphenyl)-2-(2-methoxyphenoxy)propane-1,3-diol was synthesized from 1-(4-hydroxy-3,5-dimethoxyphenyl)-2-(2-methoxyphenoxy)propane-1,3-diol (Compound 0193) by debenzylation reaction. The preparation of this compound followed the methods reported in the literature (Pardini, V.L., Smith, C.Z., Utley, J.H.P., Vargas, R.R., Viertler, H. J. Org. Chem. 1991, 56, 7305). * 1H NMR (300 MHz, CDCl3) δ: 7.14-6.90 (m, 4H), 6.68 (s, 2H, minor diastereoisomer), 6.62 (s, 2H, major diastereoisomer), 5.55 (s, 1H, minor diastereoisomer, -OH), 5.52 (s, 1H, major diastereoisomer, -OH), 4.95 (m, 1H), 4.14 (m, 1H, major diastereoisomer), 4.00 (m, 1H, minor diastereoisomer), 3.91 (s, 3H, minor diastereoisomer), 3.89 (s, 3H, major diastereoisomer), 3.88 (s, 6H, minor diastereoisomer), 3.86 (s, 6H, major diastereoisomer), 3.70-3.62 (m, 1H, major diastereoisomer). 3.70-3.62 (m, 1H, major diastereoisomer), 3.55-3.53 (m, 1H, minor diastereoisomer), 2.74 (bs, 1H). 13C NMR (75 MHz, CDCl3) Major diastereoisomers: δ 151.85, 147.32, 134.37, 131.19, 124.50, 121.89, 121.41, 112.41, 103.91, 102.9, 87.66, 73.14, 61.01, 56.58, 56.12; minor diastereoisomers: δ 151.6, 147.10, 134.71, 130.86, 124.56, 121.95, 121.31, 112.41, 103.90, 102.91, 89.74, 74.47, 61.16, 56.58, 56.14. HRMS (EI) C18H22O7NH4 [M + NH4]+ Calculated value 368.1709, measured value 368.1704.

References

[1] Patent: WO2015/138563, 2015, A1. Location in patent: Page/Page column 26
[2] Journal of the American Chemical Society, 2013, vol. 135, # 17, p. 6415 - 6418
[3] Patent: US2014/235838, 2014, A1. Location in patent: Paragraph 0070; 71; 0074; 0075

1-(4-Hydroxy-3,5-dimethoxyphenyl)-2-(2-methoxyphenoxy)propane-1,3-diol Preparation Products And Raw materials

Raw materials

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92409-34-2, 1-(4-Hydroxy-3,5-dimethoxyphenyl)-2-(2-methoxyphenoxy)propane-1,3-diolRelated Search:

1,3-Propanediol,1-(4-hydroxy-3,5-dimethoxyphenyl)-2-(2-methoxyphenoxy)-

1-(4-Hydroxy-3,5-dimethoxyphenyl)-2-(2-methoxyphenoxy)propane-1,3-diol

92409-34-2