Vanillyl ethyl ether
- Product Name
- Vanillyl ethyl ether
- CAS No.
- 13184-86-6
- Chemical Name
- Vanillyl ethyl ether
- Synonyms
- FEMA 3815;DAIRY ENHANCER;VanilinEthylEther;ETHYL VANILLYL ETHER;VANILLYL ETHYL ETHER;Vanilla alcohol ether;Xianglan alcohol ether;13184-86-6 Vanillyl ethyl ether;4-[ETHOXYMETHYL]-2-METHOXYPHENOL;Phenol, 4-(ethoxymethyl)-2-methoxy-
- CBNumber
- CB2183240
- Molecular Formula
- C10H14O3
- Formula Weight
- 182.22
- MOL File
- 13184-86-6.mol
Vanillyl ethyl ether Property
- Boiling point:
- 125°C/4mmHg(lit.)
- Density
- 1.087±0.06 g/cm3(Predicted)
- refractive index
- 1.5280 to 1.5320
- FEMA
- 3815 | VANILLYL ETHYL ETHER
- storage temp.
- Inert atmosphere,Room Temperature
- form
- clear liquid
- pka
- 9.73±0.20(Predicted)
- color
- Colorless to Almost colorless
- Odor
- at 20.00 % in ethyl alcohol. alcoholic rum sweet chocolate creamy vanilla spicy nutmeg smoky
- Odor Type
- chocolate
- JECFA Number
- 887
- LogP
- 1.46
- CAS DataBase Reference
- 13184-86-6
- NIST Chemistry Reference
- Phenol, 4-(ethoxymethyl)-2-methoxy-(13184-86-6)
- EPA Substance Registry System
- Phenol, 4-(ethoxymethyl)-2-methoxy- (13184-86-6)
Safety
- HS Code
- 2909500090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
N-Bromosuccinimide Price
- Product number
- E1028
- Product name
- 4-(Ethoxymethyl)-2-methoxyphenol
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $98
- Updated
- 2025/07/31
- Product number
- J96485
- Product name
- 4-(Ethoxymethyl)-2-methoxyphenol
- Packaging
- 5g
- Price
- $30
- Updated
- 2021/12/16
- Product number
- FFG0000629
- Product name
- VANILLYL ETHYL ETHER
- Purity
- 98.00%
- Packaging
- 5MG
- Price
- $503.05
- Updated
- 2021/12/16
- Product number
- C1174
- Product name
- 4-(Ethoxymethyl)-2-methoxyphenol
- Purity
- 97.00%
- Packaging
- 5G
- Price
- $2180
- Updated
- 2021/12/16
- Product number
- C1174
- Product name
- 4-(Ethoxymethyl)-2-methoxyphenol
- Purity
- 97.00%
- Packaging
- 25G
- Price
- $4010
- Updated
- 2021/12/16
Vanillyl ethyl ether Chemical Properties,Usage,Production
Chemical Properties
Vanillyl ethyl ether has a phenolic, smoky odor and a strong, pungent taste.
Occurrence
Reportedly present in grape brandy (cognac), rum, whiskey and vanilla.
Uses
flavors and fragrances
Definition
ChEBI: 4-(Ethoxymethyl)-2-methoxyphenol is a member of phenols and a member of methoxybenzenes.
Preparation
In a patented process, prepared by the reaction of cyclodextrin or branched-cyclodextrin with vanillyl alcohol.
Synthesis
121-33-5
122-51-0
13184-86-6
General procedure for the synthesis of vanillyl ethyl ether from vanillin and triethyl orthoformate: 3.04 g (20.0 mmol) of vanillin, 5.93 g (40.0 mmol) of triethyl orthoformate, 15.0 mg of p-toluenesulphonic acid monohydrate, and 15.0 mg 5% palladium-carbon catalyst were added to a 100 ml autoclave (equipped with an inner tube). After displacing the internal gas of the system under nitrogen protection, it was replaced with hydrogen and filled with hydrogen at 3.0 MPa. The autoclave temperature was controlled at 130°C and the reaction was continuously stirred for 1 hour. Upon completion of the reaction, the reaction mixture was cooled and the hydrogen pressure was subsequently released. The palladium carbon catalyst was removed by filtration and the unreacted triethyl orthoformate was recovered by distillation under reduced pressure, resulting in 3.60 g of vanillyl ethyl ether (97.4% purity and 96.2% yield as determined by internal standard method). The structure of the product was confirmed by 1H-NMR (CDCl3): δ=1.37 (3H, t), 3.42 (1H, q), 3.86 (3H, s), 4.44 (2H, s), 5.92 (1H, s), 6.88 (3H, m).
References
[1] Patent: EP2813482, 2014, A1. Location in patent: Paragraph 0139; 0140
Vanillyl ethyl ether Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from Vanillyl ethyl ether manufacturers
- Product
- Vanillyl ethyl ether 13184-86-6
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 1
- Release date
- 2025-09-05
- Product
- Vanillyl ethyl ether 13184-86-6
- Price
- US $50.00/kg
- Min. Order
- 1kg
- Purity
- 99
- Supply Ability
- 5000
- Release date
- 2024-11-20
- Product
- Vanillyl ethyl ether 13184-86-6
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 10ton
- Release date
- 2024-07-19