3-BROMO-2,6-DIHYDROXYBENZOIC ACID
- Product Name
- 3-BROMO-2,6-DIHYDROXYBENZOIC ACID
- CAS No.
- 26792-49-4
- Chemical Name
- 3-BROMO-2,6-DIHYDROXYBENZOIC ACID
- Synonyms
- 3-Bromo-2,6-dihydrox;3-BROMO-2,6-DIHYDROXYBE;3-BroMo-γ-resorcylic Acid;3-BROMO-2,6-DIHYDROXYBENZOIC ACID;Benzoic acid, 3-bromo-2,6-dihydroxy-
- CBNumber
- CB2248040
- Molecular Formula
- C7H5BrO4
- Formula Weight
- 233.02
- MOL File
- Mol file
3-BROMO-2,6-DIHYDROXYBENZOIC ACID Property
- Melting point:
- 198-200°C dec.
- storage temp.
- Sealed in dry,2-8°C
- solubility
- Methanol, Water
- form
- Solid
- color
- Off-White
- InChI
- InChI=1S/C7H5BrO4/c8-3-1-2-4(9)5(6(3)10)7(11)12/h1-2,9-10H,(H,11,12)
- InChIKey
- GPCLJSXGFAOJQE-UHFFFAOYSA-N
- SMILES
- C(O)(=O)C1=C(O)C=CC(Br)=C1O
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B684040
- Product name
- 3-Bromo-2,6-dihydroxybenzoicAcid
- Packaging
- 2g
- Price
- $200
- Updated
- 2021/12/16
- Product number
- B684040
- Product name
- 3-Bromo-2,6-dihydroxybenzoicAcid
- Packaging
- 5g
- Price
- $485
- Updated
- 2021/12/16
- Product number
- B684040
- Product name
- 3-Bromo-2,6-dihydroxybenzoicAcid
- Packaging
- 10g
- Price
- $810
- Updated
- 2021/12/16
- Product number
- FB19073
- Product name
- 3-Bromo-2,6-dihydroxybenzoic acid
- Packaging
- 100mg
- Price
- $50
- Updated
- 2021/12/16
- Product number
- FB19073
- Product name
- 3-Bromo-2,6-dihydroxybenzoic acid
- Packaging
- 250mg
- Price
- $100
- Updated
- 2021/12/16
3-BROMO-2,6-DIHYDROXYBENZOIC ACID Chemical Properties,Usage,Production
Chemical Properties
Off-White Solid
Synthesis
303-07-1
26792-49-4
General procedure for the synthesis of 3-bromo-2,6-dihydroxybenzoic acid from 2,6-dihydroxybenzoic acid: to a solution of the compound 2,6-dihydroxybenzoic acid (298 g, 1.93 mol, 1.0 eq.) and diisopropylamine (98 g, 0.97 mol, 0.5 eq.) in methylene chloride (3.5 L) was added batchwise N-bromosuccinimide (362 g, 2.03 mol, 1.05 eq.). 2.03 mol, 1.05 eq.) and the reaction was carried out at -78 °C. The reaction mixture was slowly warmed to room temperature and stirred for 16 h. The progress of the reaction was monitored by thin layer chromatography (TLC) until the reaction was completed. Upon completion of the reaction, the reaction mixture was evaporated to dryness and the residue was stirred in 1N hydrochloric acid (2L) for 0.5 hours. The precipitate was collected by filtration to afford the target compound 3-bromo-2,6-dihydroxybenzoic acid (370 g, 83% yield) as a light yellow solid.
References
[1] Patent: WO2016/149393, 2016, A1. Location in patent: Paragraph 0277
[2] Patent: WO2016/3929, 2016, A1. Location in patent: Paragraph 0336
[3] Journal of the Chemical Society, 1963, p. 497 - 506
3-BROMO-2,6-DIHYDROXYBENZOIC ACID Preparation Products And Raw materials
Raw materials
Preparation Products
3-BROMO-2,6-DIHYDROXYBENZOIC ACID Suppliers
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- tp@aladdinsci.com
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- United States
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View Lastest Price from 3-BROMO-2,6-DIHYDROXYBENZOIC ACID manufacturers
- Product
- 3-BROMO-2,6-DIHYDROXYBENZOIC ACID 26792-49-4
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 97.0%
- Supply Ability
- 10000KGS
- Release date
- 2025-03-07