ChemicalBook > CAS DataBase List > 3-methylmorpholine

3-methylmorpholine

Product Name
3-methylmorpholine
CAS No.
42185-06-8
Chemical Name
3-methylmorpholine
Synonyms
3-methylmorpholine;Morpholine, 3-methyl-;3-Methylmorpholine 97%;3-MethylMorpholine hcl h2o
CBNumber
CB31261195
Molecular Formula
C5H11NO
Formula Weight
101.15
MOL File
42185-06-8.mol
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3-methylmorpholine Property

Boiling point:
133-134 °C
Density 
0.9591 g/cm3(Temp: 16 °C)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
pka
9.03±0.40(Predicted)
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Safety

Hazard Codes 
Xn
Risk Statements 
22-41
Safety Statements 
26-39
RIDADR 
UN2924
HazardClass 
3, 8
HS Code 
2934999090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H225Highly Flammable liquid and vapour

H319Causes serious eye irritation

Precautionary statements

P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.

P233Keep container tightly closed.

P240Ground/bond container and receiving equipment.

P241Use explosion-proof electrical/ventilating/lighting/…/equipment.

P242Use only non-sparking tools.

P243Take precautionary measures against static discharge.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P337+P313IF eye irritation persists: Get medical advice/attention.

P370+P378In case of fire: Use … for extinction.

P403+P235Store in a well-ventilated place. Keep cool.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC
Product number
M725213
Product name
3-Methylmorpholine
Packaging
25mg
Price
$75
Updated
2021/12/16
Oakwood
Product number
093767
Product name
3-Methylmorpholine
Purity
95%
Packaging
250mg
Price
$92
Updated
2021/12/16
SynQuest Laboratories
Product number
4H56-1-98
Product name
3-Methylmorpholine
Purity
97%
Packaging
1g
Price
$112
Updated
2021/12/16
AK Scientific
Product number
W6211
Product name
3-Methylmorpholine
Packaging
1g
Price
$114
Updated
2021/12/16
Matrix Scientific
Product number
074238
Product name
3-Methylmorpholine
Purity
95+%
Packaging
250mg
Price
$231
Updated
2021/12/16
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3-methylmorpholine Chemical Properties,Usage,Production

Synthesis

1268866-46-1

42185-06-8

A solution of 4-(4-methoxybenzyl)-3-methylmorpholine (7 g, 31.53 mmol, 1.00 eq.) in methanol (70 mL) was added to a 250 mL round-bottom flask under nitrogen protection. A 10% palladium-carbon catalyst (2 g) was then added. After passing hydrogen (H2), the reaction mixture was stirred in an oil bath at 50 °C overnight. Upon completion of the reaction, the solid catalyst was removed by filtration. The filtrate was concentrated under reduced pressure to give 2.1 g (66% yield) of 3-methylmorpholine as a yellow oil.LC-MS analysis: (ES, m/z): 102 [M + H]+.

References

[1] Patent: WO2011/28947, 2011, A2. Location in patent: Page/Page column 154; 157

3-methylmorpholine Preparation Products And Raw materials

Raw materials

Preparation Products

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3-methylmorpholine Suppliers

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View Lastest Price from 3-methylmorpholine manufacturers

Hong Kong Tiansheng New Material Trading Co., Ltd
Product
3-Methylmorpholine 42185-06-8
Price
US $8.60/KG
Min. Order
1KG
Purity
98%
Supply Ability
100KG
Release date
2021-09-24
Hong Kong Tiansheng New Material Trading Co., Ltd
Product
3-Methylmorpholine 42185-06-8
Price
US $8.60/KG
Min. Order
1KG
Purity
99%
Supply Ability
1000kg
Release date
2021-11-26
Hong Kong Tiansheng New Material Trading Co., Ltd
Product
3-Methylmorpholine 42185-06-8
Price
US $8.60/KG
Min. Order
1KG
Purity
98%
Supply Ability
10KG
Release date
2021-11-26

42185-06-8, 3-methylmorpholineRelated Search:

Scopolamine hydrobromide SCOPOLAMINE METHYL NITRATE tert-Butyl (2S,3R)-(+)-6-oxo-2,3-diphenyl-4-morpholinecarboxylate Scopolamine butylbromide Anisodine hydrobromide Scopine hydrochloride PHENDIMETRAZINE BITARTRATE SCOPOLAMINE N-OXIDE HYDROBROMIDE HYOSCINE HYDROCHLORIDE Benzyl (2S,3R)-(+)-6-oxo-2,3-diphenyl-4-morpholinecarboxylate Methscopolamine bromide Benzyl (2R,3S)-(-)-6-oxo-2,3-diphenyl-4-morpholinecarboxylate tert-Butyl (2R,3S)-(-)-6-oxo-2,3-diphenyl-4-morpholinecarboxylate 2-(4-CHLORO-PHENYL)-2-METHYL-MORPHOLINE DIMETHYL-MORPHOLIN-2-YLMETHYL-AMINE (S)-2-Methylmorpholine HCl 4-BENZYL-2-(CHLOROMETHYL)MORPHOLINE 4-(4-METHYLMORPHOLINE)BENZENEBORONIC ACID, PINACOL ESTER

  • 3-methylmorpholine
  • Morpholine, 3-methyl-
  • 3-MethylMorpholine hcl h2o
  • 3-Methylmorpholine 97%
  • 42185-06-8
  • pharmacetical
  • API intermediates
  • Heterocycles