5-bromo-2-phenoxypyridine

Product Name: 5-bromo-2-phenoxypyridine
CAS No.: 59717-96-3
Chemical Name: 5-bromo-2-phenoxypyridine
Synonyms: 5-bromo-2-phenoxypyridine;Pyridine,5-bromo-2-phenoxy-
CBNumber: CB32499704
Molecular Formula: C11H8BrNO
Formula Weight: 250.09
MOL File: 59717-96-3.mol

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5-bromo-2-phenoxypyridine Property

Boiling point:: 310.0±22.0 °C(Predicted)
Density: 1.476±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 0.18±0.22(Predicted)

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B687393
Product name: 5-Bromo-2-phenoxypyridine
Packaging: 250mg
Price: $55
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB140371
Product name: 5-Bromo-2-phenoxypyridine
Packaging: 1g
Price: $55
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB140371
Product name: 5-Bromo-2-phenoxypyridine
Packaging: 2g
Price: $95
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB140371
Product name: 5-Bromo-2-phenoxypyridine
Packaging: 5G
Price: $190
Updated: 2021/12/16

AK Scientific

Product number: Z0717
Product name: 5-Bromo-2-phenoxypyridine
Packaging: 10g
Price: $244
Updated: 2021/12/16

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5-bromo-2-phenoxypyridine Chemical Properties,Usage,Production

Synthesis

624-28-2

108-95-2

59717-96-3

2,5-dibromopyridine (237 mg, 1 mmol, 1.0 equiv) and phenol (140 mg, 1.5 mmol, 1.5 equiv) were added with copper powder (32.5 mg, 0.5 mmol, 0.5 equiv), cuprous iodide (95 mg, 0.5 mmol, 0.5 equiv) and cesium carbonate (978 mg. 3.0 mmol, 3.0 equiv) in N-methylpyrrolidone (NMP, 10 mL). The reaction mixture was heated to 135 °C under nitrogen protection and maintained at this temperature for 5 h of reaction. After completion of the reaction, the solid insoluble material was removed by filtration and the filtrate was concentrated. Purification by column chromatography (eluent: ethyl acetate/petroleum ether = 10/1, v/v) afforded 5-bromo-2-phenoxypyridine as a brown solid (200 mg, 84.4% yield).

References

[1] Tetrahedron, 2013, vol. 69, # 1, p. 327 - 333
[2] Patent: CN108069974, 2018, A. Location in patent: Paragraph 0162-0165
[3] Patent: WO2018/35061, 2018, A1. Location in patent: Paragraph 0358
[4] Journal of Organometallic Chemistry, 2003, vol. 677, # 1-2, p. 57 - 72
[5] Patent: CN106146518, 2016, A. Location in patent: Paragraph 0038; 0039; 0040; 0041; 0042; 0043

5-bromo-2-phenoxypyridine Preparation Products And Raw materials

Raw materials

Preparation Products

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5-bromo-2-phenoxypyridine Suppliers

China 55 India 2 United Kingdom 2 United States 5 Global 64

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59717-96-3, 5-bromo-2-phenoxypyridineRelated Search:

5-bromo-2-phenoxypyridine

Pyridine,5-bromo-2-phenoxy-

59717-96-3