ChemicalBook > CAS DataBase List > 3,5-DibroMo-1-Methylpyridin-4(1H)-one
3,5-DibroMo-1-Methylpyridin-4(1H)-one
- Product Name
- 3,5-DibroMo-1-Methylpyridin-4(1H)-one
- CAS No.
- 2683-35-4
- Chemical Name
- 3,5-DibroMo-1-Methylpyridin-4(1H)-one
- Synonyms
- 3,5-DibroMo-1-Methylpyridin-4(1H)-one;4(1H)-Pyridinone, 3,5-dibromo-1-methyl-
- CBNumber
- CB32661651
- Molecular Formula
- C6H5Br2NO
- Formula Weight
- 266.92
- MOL File
- 2683-35-4.mol
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3,5-DibroMo-1-Methylpyridin-4(1H)-one Property
- Melting point:
- 193-194 °C
- Boiling point:
- 253.7±40.0 °C(Predicted)
- Density
- 2.130±0.06 g/cm3(Predicted)
- storage temp.
- Inert atmosphere,Room Temperature
- pka
- -2.10±0.10(Predicted)
- Appearance
- White to off-white Solid
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N-Bromosuccinimide Price
Biosynth Carbosynth
- Product number
- FD141309
- Product name
- 3,5-Dibromo-1-methylpyridin-4(1H)-one
- Packaging
- 250mg
- Price
- $57.5
- Updated
- 2021/12/16
Biosynth Carbosynth
- Product number
- FD141309
- Product name
- 3,5-Dibromo-1-methylpyridin-4(1H)-one
- Packaging
- 500mg
- Price
- $100
- Updated
- 2021/12/16
Biosynth Carbosynth
- Product number
- FD141309
- Product name
- 3,5-Dibromo-1-methylpyridin-4(1H)-one
- Packaging
- 1g
- Price
- $175
- Updated
- 2021/12/16
Biosynth Carbosynth
- Product number
- FD141309
- Product name
- 3,5-Dibromo-1-methylpyridin-4(1H)-one
- Packaging
- 2g
- Price
- $298
- Updated
- 2021/12/16
Matrix Scientific
- Product number
- 126317
- Product name
- 3,5-Dibromo-1-methylpyridin-4(1H)-one
- Purity
- >95%
- Packaging
- 1g
- Price
- $360
- Updated
- 2021/12/16
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3,5-DibroMo-1-Methylpyridin-4(1H)-one Chemical Properties,Usage,Production
Synthesis
25813-24-5
74-88-4
2683-35-4
General method: Iodomethane (4 mmol, 2 eq.) was added to a solution of 3,5-dibromo-4-methoxypyridine (2 mmol) dissolved in different solvents (15 mL) and the mixture was refluxed overnight. The reaction progress was monitored by thin layer chromatography (TLC). Upon completion of the reaction, the solvent was removed by distillation under reduced pressure and the residue was purified by column chromatography (eluent ratio: ethyl acetate/methanol, 20:1→5:1) to afford the target product 3,5-dibromo-1-methylpyridin-4(1H)-one.
References
[1] Synthetic Communications, 2017, vol. 47, # 9, p. 872 - 877
3,5-DibroMo-1-Methylpyridin-4(1H)-one Preparation Products And Raw materials
Raw materials
Preparation Products
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3,5-DibroMo-1-Methylpyridin-4(1H)-one Suppliers
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