ChemicalBook > CAS DataBase List > 3,5-DibroMo-1-Methylpyridin-4(1H)-one

3,5-DibroMo-1-Methylpyridin-4(1H)-one

Product Name
3,5-DibroMo-1-Methylpyridin-4(1H)-one
CAS No.
2683-35-4
Chemical Name
3,5-DibroMo-1-Methylpyridin-4(1H)-one
Synonyms
3,5-DibroMo-1-Methylpyridin-4(1H)-one;4(1H)-Pyridinone, 3,5-dibromo-1-methyl-
CBNumber
CB32661651
Molecular Formula
C6H5Br2NO
Formula Weight
266.92
MOL File
2683-35-4.mol
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3,5-DibroMo-1-Methylpyridin-4(1H)-one Property

Melting point:
193-194 °C
Boiling point:
253.7±40.0 °C(Predicted)
Density 
2.130±0.06 g/cm3(Predicted)
storage temp. 
Inert atmosphere,Room Temperature
pka
-2.10±0.10(Predicted)
Appearance
White to off-white Solid
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

Biosynth Carbosynth
Product number
FD141309
Product name
3,5-Dibromo-1-methylpyridin-4(1H)-one
Packaging
250mg
Price
$57.5
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD141309
Product name
3,5-Dibromo-1-methylpyridin-4(1H)-one
Packaging
500mg
Price
$100
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD141309
Product name
3,5-Dibromo-1-methylpyridin-4(1H)-one
Packaging
1g
Price
$175
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD141309
Product name
3,5-Dibromo-1-methylpyridin-4(1H)-one
Packaging
2g
Price
$298
Updated
2021/12/16
Matrix Scientific
Product number
126317
Product name
3,5-Dibromo-1-methylpyridin-4(1H)-one
Purity
>95%
Packaging
1g
Price
$360
Updated
2021/12/16
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3,5-DibroMo-1-Methylpyridin-4(1H)-one Chemical Properties,Usage,Production

Synthesis

25813-24-5

74-88-4

2683-35-4

General method: Iodomethane (4 mmol, 2 eq.) was added to a solution of 3,5-dibromo-4-methoxypyridine (2 mmol) dissolved in different solvents (15 mL) and the mixture was refluxed overnight. The reaction progress was monitored by thin layer chromatography (TLC). Upon completion of the reaction, the solvent was removed by distillation under reduced pressure and the residue was purified by column chromatography (eluent ratio: ethyl acetate/methanol, 20:1→5:1) to afford the target product 3,5-dibromo-1-methylpyridin-4(1H)-one.

References

[1] Synthetic Communications, 2017, vol. 47, # 9, p. 872 - 877

3,5-DibroMo-1-Methylpyridin-4(1H)-one Preparation Products And Raw materials

Raw materials

Preparation Products

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3,5-DibroMo-1-Methylpyridin-4(1H)-one Suppliers

Carbosynth
Tel
--
Fax
--
Email
sales@carbosynth.com
Country
United Kingdom
ProdList
6005
Advantage
58

2683-35-4, 3,5-DibroMo-1-Methylpyridin-4(1H)-oneRelated Search:


  • 3,5-DibroMo-1-Methylpyridin-4(1H)-one
  • 4(1H)-Pyridinone, 3,5-dibromo-1-methyl-
  • 2683-35-4