methyl 4-amino-2-ethylbenzoate

Product Name: methyl 4-amino-2-ethylbenzoate
CAS No.: 1211589-24-0
Chemical Name: methyl 4-amino-2-ethylbenzoate
Synonyms: methyl 4-amino-2-ethylbenzoate;Benzoic acid, 4-amino-2-ethyl-, methyl ester
CBNumber: CB34632538
Molecular Formula: C10H13NO2
Formula Weight: 179.22
MOL File: 1211589-24-0.mol

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methyl 4-amino-2-ethylbenzoate Property

Boiling point:: 325.3±30.0 °C(Predicted)
Density: 1.103±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 2.60±0.10(Predicted)
Appearance: Light yellow to yellow Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H312Harmful in contact with skin

H332Harmful if inhaled

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

AK Scientific

Product number: 6868DN
Product name: Methyl4-amino-2-ethylbenzoate
Packaging: 5g
Price: $728
Updated: 2021/12/16

Crysdot

Product number: CD12189851
Product name: Methyl4-amino-2-ethylbenzoate
Purity: 95%
Packaging: 100mg
Price: $33
Updated: 2021/12/16

Ambeed

Product number: A126773
Product name: Methyl4-amino-2-ethylbenzoate
Purity: 95%
Packaging: 100mg
Price: $36
Updated: 2021/12/16

Crysdot

Product number: CD12189851
Product name: Methyl4-amino-2-ethylbenzoate
Purity: 95%
Packaging: 250mg
Price: $50
Updated: 2021/12/16

Ambeed

Product number: A126773
Product name: Methyl4-amino-2-ethylbenzoate
Purity: 95%
Packaging: 250mg
Price: $52
Updated: 2021/12/16

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methyl 4-amino-2-ethylbenzoate Chemical Properties,Usage,Production

Synthesis

959778-15-5

1211589-24-0

Stage 2: Synthesis of methyl 4-amino-2-ethylbenzoate 15.0 g (72.3 mmol) of methyl 4-nitro-2-vinylbenzoate was dissolved in 150 mL of methanol and placed in an autoclave and subjected to a hydrogenation reaction for 15 h at 5 bar hydrogen pressure. Upon completion of the reaction, the reaction solution was filtered through diatomaceous earth to remove the catalyst. Subsequently, the solvent was removed by distillation under reduced pressure to obtain the crude product. The crude product was purified by silica gel column chromatography using cyclohexane/ethyl acetate (3:1, v/v) as eluent. Finally, 2.4 g (24% yield) of the target compound methyl 4-amino-2-ethylbenzoate was obtained. The product was analyzed by HPLC/MS showing: logP = 1.84; mass spectrum (m/z): 180.2 ([M+H]+). 1H NMR (CD3CN) data were as follows: δ 1.14 (t, 3H), 2.88 (q, 2H), 3.75 (s, 3H), 4.60 (br.s, 2H), 6.45-6.50 (m, 2H). 7.68 (d, 1H).

References

[1] Patent: US2014/88167, 2014, A1. Location in patent: Paragraph 0558; 0559; 0560

methyl 4-amino-2-ethylbenzoate Preparation Products And Raw materials

Raw materials

Preparation Products

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1211589-24-0, methyl 4-amino-2-ethylbenzoateRelated Search:

methyl 4-amino-2-ethylbenzoate

Benzoic acid, 4-amino-2-ethyl-, methyl ester

1211589-24-0