PENTAERYTHRITOL TRICHLOROHYDRIN

Product Name: PENTAERYTHRITOL TRICHLOROHYDRIN
CAS No.: 813-99-0
Chemical Name: PENTAERYTHRITOL TRICHLOROHYDRIN
Synonyms: Pentaerythrityl trichlorohydrin;PENTAERYTHRITOL TRICHLOROHYDRIN;2,2,2-TRIS-(CHLOROMETHYL)-ETHANOL;3-CHLORO-2,2-DICHLOROMETHYLPROPANOL;3-Chloro-2,2-bis(chloromethyl)propan-1-ol;2,2-bis(chloromethyl)-3-chloro-1-propanol;3- CHLORO-2,2-BIS(CHLOROMETHYL)-1-PROPANOL;1-Propanol,3-chloro-2,2-bis(chloromethyl)-;3-Chloro-2,2-bis(chloromethyl) propan-1-ol (Pentaerythrityl trichlorohydrin)
CBNumber: CB3767117
Molecular Formula: C5H9Cl3O
Formula Weight: 191.48
MOL File: 813-99-0.mol

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PENTAERYTHRITOL TRICHLOROHYDRIN Property

Melting point:: 80 °C
Boiling point:: 274.39°C (rough estimate)
Density: 1.4096 (rough estimate)
refractive index: 1.5300 (estimate)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 13.83±0.10(Predicted)
InChI: InChI=1S/C5H9Cl3O/c6-1-5(2-7,3-8)4-9/h9H,1-4H2
InChIKey: VRWHPVMGJTYPLS-UHFFFAOYSA-N
SMILES: C(O)C(CCl)(CCl)CCl

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Safety

HS Code: 2905599890

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H318Causes serious eye damage

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: S551198
Product name: 2,2,2-TRIS-(CHLOROMETHYL)-ETHANOL
Purity: Aldrich<sup>CPR</sup>
Packaging: 1 unit
Price: $185
Updated: 2025/07/31

Sigma-Aldrich

Product number: S551198
Product name: 2,2,2-TRIS-(CHLOROMETHYL)-ETHANOL
Purity: AldrichCPR
Packaging: 250MG
Price: $179
Updated: 2024/03/01

TRC

Product number: C609745
Product name: 3-Chloro-2,2-bis(chloromethyl)propan-1-ol
Packaging: 2.5g
Price: $75
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2101-5-02
Product name: 3-Chloro-2,2-bis(chloromethyl)propan-1-ol
Packaging: 5G
Price: $100
Updated: 2021/12/16

AK Scientific

Product number: 0075AF
Product name: 3-Chloro-2,2-bis(chloromethyl)propan-1-ol
Packaging: 5g
Price: $131
Updated: 2021/12/16

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PENTAERYTHRITOL TRICHLOROHYDRIN Chemical Properties,Usage,Production

Synthesis

115-77-5

813-99-0

The general procedure for the synthesis of 3-chloro-2,2-dichloromethylpropan-1-ol from pentaerythritol was as follows: pentaerythritol (15 g, 0.11 mol) was dissolved in pyridine (27 ml) and heated to 65 °C. Thionyl chloride (24.7 ml, 0.33 mol) was added slowly and dropwise over a period of 4 h. The temperature of the reaction was controlled to be between 65°C and 95°C. After completion of the reaction, the reaction mixture was continued to be stirred at 50 °C for 18 hours. Subsequently, the reaction solution was heated to 120 °C-130 °C for concentration and then cooled to room temperature. The concentrated reaction solution was slowly poured into ice water (75 ml) and stirred for 30 minutes. The resulting solid product was collected by filtration, washed well with water and dried to give 3-chloro-2,2-bis(chloromethyl)propan-1-ol (15.4 g, 73% yield).

References

[1] Patent: KR101592370, 2016, B1. Location in patent: Paragraph 0204; 0205; 0206; 0207
[2] Australian Journal of Chemistry, 1988, vol. 41, # 12, p. 1953 - 1962
[3] Patent: US2835709, 1955,
[4] Mededelingen van de Koninklijke Vlaamse Academie voor Wetenschappen, Letteren en Schone Kunsten van Belgie, Klasse der Wetenschappen, 1940, vol. 2, # 5, p. 3,16
[5] Patent: US2835709, 1955,

PENTAERYTHRITOL TRICHLOROHYDRIN Preparation Products And Raw materials

Raw materials

Preparation Products

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PENTAERYTHRITOL TRICHLOROHYDRIN Suppliers

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View Lastest Price from PENTAERYTHRITOL TRICHLOROHYDRIN manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD

Product: pentaerythritol trichlorohydrin 813-99-0
Price: US $2.00-6.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 100kg
Release date: 2025-08-08

813-99-0, PENTAERYTHRITOL TRICHLOROHYDRINRelated Search:

AURORA KA-1416 3-Chloro-2,2-dimethyl-1-propanol 1-CHLORO-2,2-DIMETHYLPROPANE 2,2-Dimethyl-1,3-dichloropropane 3-CHLORO-2,2-DICHLOROMETHYL PROPIONIC ACID PENTAERYTHRITOL TRICHLOROHYDRIN 1,1,1-TRIS(CHLOROMETHYL)ETHANE

3- CHLORO-2,2-BIS(CHLOROMETHYL)-1-PROPANOL

3-CHLORO-2,2-DICHLOROMETHYLPROPANOL

PENTAERYTHRITOL TRICHLOROHYDRIN

2,2-bis(chloromethyl)-3-chloro-1-propanol

Pentaerythrityl trichlorohydrin

3-Chloro-2,2-bis(chloromethyl)propan-1-ol

1-Propanol,3-chloro-2,2-bis(chloromethyl)-

3-Chloro-2,2-bis(chloromethyl) propan-1-ol (Pentaerythrityl trichlorohydrin)

2,2,2-TRIS-(CHLOROMETHYL)-ETHANOL

813-99-0

C5H9Cl3O