Methyl2-Amino-4-Iodobenzoate
- Product Name
- Methyl2-Amino-4-Iodobenzoate
- CAS No.
- 144550-76-5
- Chemical Name
- Methyl2-Amino-4-Iodobenzoate
- Synonyms
- Methyl2-Amino-4-Iodobenzoate;Benzoic acid, 2-amino-4-iodo-, methyl ester
- CBNumber
- CB41028131
- Molecular Formula
- C8H8INO2
- Formula Weight
- 277.06
- MOL File
- 144550-76-5.mol
Methyl2-Amino-4-Iodobenzoate Property
- Melting point:
- 71-73 °C
- Boiling point:
- 337.7±32.0 °C(Predicted)
- Density
- 1.826±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 1.39±0.10(Predicted)
- Appearance
- Light yellow to yellow Solid
N-Bromosuccinimide Price
- Product number
- 7124AA
- Product name
- Methyl2-amino-4-iodobenzoate
- Packaging
- 5g
- Price
- $394
- Updated
- 2021/12/16
- Product number
- HCH0369137
- Product name
- METHYL-2-AMINO-4-IODOBENZOATE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $502.96
- Updated
- 2021/12/16
- Product number
- 7124AA
- Product name
- Methyl2-amino-4-iodobenzoate
- Packaging
- 25g
- Price
- $1538
- Updated
- 2021/12/16
- Product number
- 144550765
- Product name
- Methyl2-amino-4-iodobenzoate
- Packaging
- 1g
- Price
- $1579.4
- Updated
- 2021/12/16
- Product number
- 61-3392
- Product name
- Methyl2-amino-4-iodobenzoate
- Purity
- 95%-98%
- Packaging
- 25g
- Price
- $1620
- Updated
- 2021/12/16
Methyl2-Amino-4-Iodobenzoate Chemical Properties,Usage,Production
Synthesis
67-56-1
117324-10-4
144550-76-5
General procedure for the synthesis of methyl 2-amino-4-iodobenzoate from methanol and 2-acetamido-4-iodobenzoic acid (CAS:117324-10-4): 16.1 g of 2-acetamido-4-iodobenzoic acid (melting point 233°C-235°C; synthesized according to U.S. Patent 4,762,838) was dissolved in 325 ml of anhydrous methanol, cooled to 0°C and passed through a dry hydrogen chloride gas to saturation. The reaction mixture was heated to reflux for 15 hours, cooled to room temperature and again passed through dry HCl gas to saturation, followed by standing at room temperature for 24 hours. Upon completion of the reaction, the solvent was removed by distillation under reduced pressure and the residue was dissolved in dichloromethane. The organic phase was washed to neutrality with saturated aqueous sodium bicarbonate to remove unreacted acid. The organic phase was dried over anhydrous sodium sulfate and concentrated under reduced pressure to give 13.8 g of methyl 2-amino-4-iodobenzoate with a melting point of 63°C-67°C.
References
[1] Patent: WO2006/41773, 2006, A2. Location in patent: Page/Page column 303-304
[2] Patent: US2017/121294, 2017, A1. Location in patent: Paragraph 0058
Methyl2-Amino-4-Iodobenzoate Preparation Products And Raw materials
Raw materials
Preparation Products
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