2-methylsulfanylpyrimidine-4-carbonitrile
- Product Name
- 2-methylsulfanylpyrimidine-4-carbonitrile
- CAS No.
- 1124-75-0
- Chemical Name
- 2-methylsulfanylpyrimidine-4-carbonitrile
- Synonyms
- 2-(Methylthio)pyriMidine-4-carbonitrile;2-(Methylthio)-4-pyrimidinecarbonitrile;4-Pyrimidinecarbonitrile, 2-(methylthio)-;2-methylsulfanylpyrimidine-4-carbonitrile
- CBNumber
- CB51518655
- Molecular Formula
- C6H5N3S
- Formula Weight
- 151.19
- MOL File
- 1124-75-0.mol
2-methylsulfanylpyrimidine-4-carbonitrile Property
- storage temp.
- 2-8°C
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M725705
- Product name
- 2-(Methylthio)-4-pyrimidinecarbonitrile
- Packaging
- 100mg
- Price
- $175
- Updated
- 2021/12/16
- Product number
- X9012
- Product name
- 2-(Methylthio)pyrimidine-4-carbonitrile
- Packaging
- 1g
- Price
- $478
- Updated
- 2021/12/16
- Product number
- CHM0294853
- Product name
- 2-(METHYLTHIO)-4-PYRIMIDINECARBONITRILE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $504.46
- Updated
- 2021/12/16
- Product number
- X9012
- Product name
- 2-(Methylthio)pyrimidine-4-carbonitrile
- Packaging
- 250mg
- Price
- $227
- Updated
- 2021/12/16
- Product number
- 076241
- Product name
- 2-(Methylthio)-4-pyrimidinecarbonitrile
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $537
- Updated
- 2021/12/16
2-methylsulfanylpyrimidine-4-carbonitrile Chemical Properties,Usage,Production
Synthesis
544-92-3
1122-74-3
1124-75-0
A. 4-Iodo-2-methylsulfonylpyrimidine (7 g, 27.5 mmol) and cuprous cyanide (2.46 g, 27.5 mmol) were dissolved in pyridine (150 mL) and heated to reflux for 4 hours. Upon completion of the reaction, the mixture was cooled to room temperature, the reaction solution was concentrated, filtered, and the solids were washed with ether. The filtrate was washed sequentially with water and brine, dried over anhydrous sodium sulfate, filtered and concentrated. The residue was purified by silica gel column chromatography with 10% ethyl acetate-hexane as eluent to give 2-(methylthio)-4-pyrimidinecarbonitrile (3.2 g, 77% yield) as a white solid. Mass spectrum (electrospray positive ion mode) m/z 152 [M + H]+.
References
[1] Patent: WO2006/9889, 2006, A1. Location in patent: Page/Page column 56
2-methylsulfanylpyrimidine-4-carbonitrile Preparation Products And Raw materials
Raw materials
Preparation Products
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