6-BroMopyridine-2-sulfonaMide
- Product Name
- 6-BroMopyridine-2-sulfonaMide
- CAS No.
- 856013-04-2
- Chemical Name
- 6-BroMopyridine-2-sulfonaMide
- Synonyms
- 6-BroMopyridine-2-sulfonaMide;2-Pyridinesulfonamide, 6-bromo-
- CBNumber
- CB52628672
- Molecular Formula
- C5H5BrN2O2S
- Formula Weight
- 237.07
- MOL File
- 856013-04-2.mol
6-BroMopyridine-2-sulfonaMide Property
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- Appearance
- Light yellow to yellow Solid
N-Bromosuccinimide Price
- Product number
- FB141691
- Product name
- 6-Bromopyridine-2-sulfonamide
- Packaging
- 50mg
- Price
- $51
- Updated
- 2021/12/16
- Product number
- FB141691
- Product name
- 6-Bromopyridine-2-sulfonamide
- Packaging
- 100mg
- Price
- $89
- Updated
- 2021/12/16
- Product number
- FB141691
- Product name
- 6-Bromopyridine-2-sulfonamide
- Packaging
- 250mg
- Price
- $177.5
- Updated
- 2021/12/16
- Product number
- HCH0367861
- Product name
- 6-BROMOPYRIDINE-2-SULFONAMIDE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $500.27
- Updated
- 2021/12/16
- Product number
- 3298AC
- Product name
- 6-Bromopyridine-2-sulfonamide
- Packaging
- 1g
- Price
- $533
- Updated
- 2021/12/16
6-BroMopyridine-2-sulfonaMide Chemical Properties,Usage,Production
Synthesis
1135871-89-4
856013-04-2
b) 6-Bromo-N-(tert-butyl)pyridine-2-sulfonamide (478 mg, 1.63 mmol) was dissolved in trifluoroacetic acid (TFA, 2 mL), and the reaction mixture was stirred for 3 hours at 60 °C. After completion of the reaction, TFA was evaporated under reduced pressure and the residue was treated with a solvent mixture of petroleum ether and ethyl ether (Et2O) to precipitate a brown solid. The solid was collected by filtration and ground three times with ether to give the final white solid product 6-bromopyridine-2-sulfonamide (125 mg, 32% yield). The product was characterized by 1H NMR (DMSO-d6, ppm): 7.98 (t, J=7.5 Hz, 1H), 7.91 (dd, J=7.5 and 1.2 Hz, 1H), 7.87 (dd, J=7.5 and 0.9 Hz, 1H).
References
[1] Patent: WO2009/39553, 2009, A1. Location in patent: Page/Page column 87
6-BroMopyridine-2-sulfonaMide Preparation Products And Raw materials
Raw materials
Preparation Products
6-BroMopyridine-2-sulfonaMide Suppliers
- Tel
- --
- Fax
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- sales@carbosynth.com
- Country
- United Kingdom
- ProdList
- 6005
- Advantage
- 58