3-ETHYLPHENYLBORONIC ACID
- Product Name
- 3-ETHYLPHENYLBORONIC ACID
- CAS No.
- 90555-65-0
- Chemical Name
- 3-ETHYLPHENYLBORONIC ACID
- Synonyms
- 3-Ethylphenylboronic;3-Ethylphenylboronicaci;3-ETHYLPHENYLBORONIC ACID;3-Ethylbenzeneboronic acid;B-(3-Ethylphenyl)-Boronic Acid;Boronic acid,b-(3-ethylphenyl)-;3-Ethylphenylboronic acid - [E2596];3-ETHYLPHENYLBORONIKeyUp "Alt", 1 C ACID
- CBNumber
- CB5487640
- Molecular Formula
- C8H11BO2
- Formula Weight
- 149.98
- MOL File
- 90555-65-0.mol
3-ETHYLPHENYLBORONIC ACID Property
- Melting point:
- 102.5-107.5 C
- Boiling point:
- 299.6±33.0 °C(Predicted)
- Density
- 1.07±0.1 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- pka
- 8.62±0.10(Predicted)
- form
- solid
- color
- White
Safety
- Hazard Codes
- Xi
- Risk Statements
- 36/37/38-36/38
- Safety Statements
- 26-36/37
- WGK Germany
- 3
- HS Code
- 2931900090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
N-Bromosuccinimide Price
- Product number
- SYX00037
- Product name
- 3-Ethylphenylboronic acid
- Purity
- Aldrich
- Packaging
- 1g
- Price
- $216
- Updated
- 2025/07/31
- Product number
- E926093
- Product name
- 3-Ethylphenylboronic acid
- Packaging
- 250mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 092255
- Product name
- 3-Ethylphenylboronic acid
- Purity
- 97%
- Packaging
- 100mg
- Price
- $30
- Updated
- 2021/12/16
- Product number
- CS-W005541
- Product name
- 3-Ethylphenylboronic acid
- Packaging
- 1g
- Price
- $85
- Updated
- 2021/12/16
- Product number
- 6760-1-82
- Product name
- 3-Ethylphenylboronic acid
- Purity
- 97%
- Packaging
- 1g
- Price
- $114
- Updated
- 2021/12/16
3-ETHYLPHENYLBORONIC ACID Chemical Properties,Usage,Production
Synthesis
2725-82-8
90555-65-0
The general procedure for the synthesis of 3-ethylphenylboronic acid from 3-bromoethylbenzene was as follows: 1-bromo-3-ethylbenzene (2.80 g, 15 mmol) was dissolved in tetrahydrofuran (40 mL) under nitrogen protection, cooled to -78 °C and stirred. n-Butyllithium (10 mL, 16 mmol) was slowly added and stirring was continued for 10 minutes. Subsequently, triisopropyl borate (6.92 mL, 30 mmol) was added and the reaction mixture was allowed to gradually warm to room temperature. Upon completion of the reaction, 1 M hydrochloric acid (50 mL) was added for acidification and then extracted with ether (100 mL). The organic phase was dried with anhydrous sodium sulfate, filtered and concentrated. The crude product was purified by recrystallization in water and washed with hexane to give 0.591 g of 3-ethylphenylboronic acid in 26% yield. Mass spectrometry analysis showed (M + ACN)+ peak of 195.
References
[1] Journal of Organic Chemistry, 2000, vol. 65, # 10, p. 3200 - 3206
[2] Patent: WO2006/9876, 2006, A2. Location in patent: Page/Page column 183
3-ETHYLPHENYLBORONIC ACID Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-ETHYLPHENYLBORONIC ACID manufacturers
- Product
- 3-ETHYLPHENYLBORONIC ACID 90555-65-0
- Price
- US $34.00-1.20/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2024-04-08
- Product
- 3-ETHYLPHENYLBORONIC ACID 90555-65-0
- Price
- US $1.00/KG
- Min. Order
- 1ASSAYS
- Purity
- 99%
- Supply Ability
- 200kg
- Release date
- 2020-01-02