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tert-butyl(3-hydroxyphenethyl)carbamate

Product Name
tert-butyl(3-hydroxyphenethyl)carbamate
CAS No.
129150-68-1
Chemical Name
tert-butyl(3-hydroxyphenethyl)carbamate
Synonyms
3-[2-(Boc-amino)ethyl]phenol;tert-butyl(3-hydroxyphenethyl)carbamate;tert-Butyl N-(3-hydroxyphenethyl)carbamate;tert-butyl N-[2-(3-hydroxyphenyl)ethyl]carbamate;N-(t-butoxycarbonyl)-2-(3-hydroxyphenyl)-ethylamine;Carbamic acid, N-[2-(3-hydroxyphenyl)ethyl]-, 1,1-dimethylethyl ester
CBNumber
CB63144006
Molecular Formula
C13H19NO3
Formula Weight
237.29
MOL File
129150-68-1.mol
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tert-butyl(3-hydroxyphenethyl)carbamate Property

Boiling point:
397.1±25.0 °C(Predicted)
Density 
1.100±0.06 g/cm3(Predicted)
storage temp. 
2-8°C
pka
9.98±0.10(Predicted)
Appearance
Off-white to light yellow Solid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific
Product number
1984AQ
Product name
tert-butyl3-hydroxyphenethylcarbamate
Packaging
250mg
Price
$333.2
Updated
2021/12/16
Chemenu
Product number
CM248716
Product name
tert-Butyl3-hydroxyphenethylcarbamate
Purity
95+%
Packaging
5g
Price
$880
Updated
2021/12/16
Alichem
Product number
129150681
Product name
tert-Butyl3-hydroxyphenethylcarbamate
Packaging
5g
Price
$931.59
Updated
2021/12/16
Ambeed
Product number
A101127
Product name
tert-Butyl3-hydroxyphenethylcarbamate
Purity
97%
Packaging
100mg
Price
$66
Updated
2021/12/16
Crysdot
Product number
CD12155457
Product name
tert-Butyl3-hydroxyphenethylcarbamate
Purity
97%
Packaging
1g
Price
$265
Updated
2021/12/16
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tert-butyl(3-hydroxyphenethyl)carbamate Chemical Properties,Usage,Production

Synthesis

132513-29-2

129150-68-1

Step B: Synthesis of tert-butyl [2-(3-hydroxyphenyl)ethyl]carbamate; 1 g of 10% Pd/C catalyst was added to a 100 mL ethanol solution containing 13 g (0.039 mol) of tert-butyl [2-(3-benzyloxyphenyl)ethyl]carbamate. The reaction mixture was subjected to hydrogenation at 40 psi hydrogen pressure overnight. Upon completion of the reaction, the catalyst was removed by filtration and washed with ethanol. Subsequently, the solvent was evaporated under reduced pressure to give 9.4 g of tert-butyl 3-hydroxyphenethylcarbamate as a colorless oil in quantitative yield.1H-NMR (CDCl3) δ: 7.22-7.12 (m, 1H); 6.78-6.66 (m, 3H); 4.56 (bs, 1H); 3.42-3.30 (m, 2H); 2.74 (t, 2H); 1.44 (s, 9H).

References

[1] Patent: WO2007/71311, 2007, A1. Location in patent: Page/Page column 55-56
[2] Patent: WO2014/95920, 2014, A1. Location in patent: Page/Page column 70
[3] Journal of Organic Chemistry, 1990, vol. 55, # 24, p. 6000 - 6017
[4] Patent: WO2009/68177, 2009, A1. Location in patent: Page/Page column 39
[5] Patent: US2010/210631, 2010, A1. Location in patent: Page/Page column 14

tert-butyl(3-hydroxyphenethyl)carbamate Preparation Products And Raw materials

Raw materials

Preparation Products

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tert-butyl(3-hydroxyphenethyl)carbamate Suppliers

China 22 India 1 United States 1 Global 24
A.J Chemicals
Tel
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Fax
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Email
sales@ajchem.in
Country
India
ProdList
6100
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129150-68-1, tert-butyl(3-hydroxyphenethyl)carbamateRelated Search:

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  • tert-butyl(3-hydroxyphenethyl)carbamate
  • N-(t-butoxycarbonyl)-2-(3-hydroxyphenyl)-ethylamine
  • 3-[2-(Boc-amino)ethyl]phenol
  • Carbamic acid, N-[2-(3-hydroxyphenyl)ethyl]-, 1,1-dimethylethyl ester
  • tert-butyl N-[2-(3-hydroxyphenyl)ethyl]carbamate
  • tert-Butyl N-(3-hydroxyphenethyl)carbamate
  • 129150-68-1