ChemicalBook > CAS DataBase List > 2-(4-METHYLPIPERAZINO)BENZALDEHYDE

2-(4-METHYLPIPERAZINO)BENZALDEHYDE

Product Name
2-(4-METHYLPIPERAZINO)BENZALDEHYDE
CAS No.
85803-62-9
Chemical Name
2-(4-METHYLPIPERAZINO)BENZALDEHYDE
Synonyms
BUTTPARK 33\06-51;2-(4-Methylpiperazino)benzadehyde;2-(4-METHYLPIPERAZINO)BENZALDEHYDE;2-(4-METHYLPIPERAZIN-1-YL)BENZALDEHYDE;2-(4-Methyl-1-piperazinyl)benzaldehyde;Benzaldehyde, 2-(4-methyl-1-piperazinyl)-;2-(4-methyl-1-piperazin-4-iumyl)benzaldehyde
CBNumber
CB6369404
Molecular Formula
C12H16N2O
Formula Weight
204.27
MOL File
85803-62-9.mol
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2-(4-METHYLPIPERAZINO)BENZALDEHYDE Property

Melting point:
44 °C
Boiling point:
110
Density 
1.107±0.06 g/cm3(Predicted)
storage temp. 
2-8°C
pka
7.69±0.42(Predicted)
Appearance
Colorless to light yellow Liquid
CAS DataBase Reference
85803-62-9(CAS DataBase Reference)
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Safety

Hazard Codes 
C,Xi
Risk Statements 
36/37/38-36
Safety Statements 
26-36/37/39
Hazard Note 
Corrosive
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

TRC
Product number
M331610
Product name
2-(4-Methylpiperazin-1-yl)benzaldehyde
Packaging
100mg
Price
$45
Updated
2021/12/16
AK Scientific
Product number
Y4337
Product name
2-(4-Methylpiperazin-1-yl)benzaldehyde
Packaging
250mg
Price
$76
Updated
2021/12/16
AK Scientific
Product number
Y4337
Product name
2-(4-Methylpiperazin-1-yl)benzaldehyde
Packaging
5g
Price
$247
Updated
2021/12/16
Matrix Scientific
Product number
081567
Product name
2-(4-Methylpiperazino)benzadehyde
Purity
97%
Packaging
1g
Price
$213
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0960420
Product name
2-(4-METHYLPIPERAZIN-1-YL)BENZALDEHYDE
Purity
95.00%
Packaging
250MG
Price
$615.34
Updated
2021/12/16
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2-(4-METHYLPIPERAZINO)BENZALDEHYDE Chemical Properties,Usage,Production

Synthesis

109-01-3

446-52-6

85803-62-9

General procedure: 2-fluorobenzaldehyde (20.0 mL, 189.9 mmol), 1-methylpiperazine (33.0 mL, 297.7 mmol) and potassium carbonate (40.0 g, 289.4 mmol) were dissolved in water (200 mL) and heated to reflux. After the reaction was completed, it was cooled to room temperature and the reaction mixture was extracted with ethyl acetate (2 x 150 mL). The organic phases were combined, washed with brine, dried over anhydrous magnesium sulfate, and concentrated under reduced pressure to afford the target product 2-(4-methylpiperazine)benzaldehyde (PP57, 38.6 g, 100%) as an orange oil. Its NMR hydrogen spectrum (CDCl3) data were as follows: δ 10.10 (s, 1H), 7.77 (dd, J = 7.9, 1.7 Hz, 1H), 7.51-7.48 (m, 1H), 7.10-7.06 (m, 2H), 3.11 (t, J = 4.6 Hz, 4H), 2.63 (br s, 4H), 2.36 (s, 3H) .

References

[1] Patent: WO2006/48727, 2006, A1. Location in patent: Page/Page column 83
[2] Patent: US2003/87914, 2003, A1
[3] Russian Chemical Bulletin, 2004, vol. 53, # 6, p. 1240 - 1247
[4] Chemical Communications, 2017, vol. 53, # 75, p. 10448 - 10451
[5] Synthesis, 1987, # 7, p. 641 - 645

2-(4-METHYLPIPERAZINO)BENZALDEHYDE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-(4-METHYLPIPERAZINO)BENZALDEHYDE Suppliers

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View Lastest Price from 2-(4-METHYLPIPERAZINO)BENZALDEHYDE manufacturers

Career Henan Chemical Co
Product
2-(4-METHYLPIPERAZINO)BENZALDEHYDE 85803-62-9
Price
US $3.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
100kg
Release date
2019-07-04

85803-62-9, 2-(4-METHYLPIPERAZINO)BENZALDEHYDERelated Search:

2-(4-METHYL-PIPERAZIN-1-YL)-BENZOIC ACID 1-Boc-4-(2-formylphenyl)piperazine 2-(4-METHYLPIPERAZINO)BENZALDEHYDE 4-(4-METHYLPIPERAZINO)BENZALDEHYDE 2-(4-[5-(TRIFLUOROMETHYL)-2-PYRIDYL]PIPERAZINO)BENZALDEHYDE 1-BOC-4-(2-CARBOXYPHENYL)PIPERAZINE 2-(4-ETHYLPIPERAZIN-1-YL)BENZALDEHYDE 2-(4-BENZYLPIPERAZINO)BENZALDEHYDE 5-AMINO-2-(4-METHYL-PIPERAZIN-1-YL)-BENZOIC ACID METHYL 5-AMINO-2-(4-BENZYLPIPERAZINO)BENZENECARBOXYLATE 2-(4-methylpiperazino)-5-nitrobenzenecarbaldehyde METHYL 2-(4-BENZYLPIPERAZINO)-5-NITROBENZENECARBOXYLATE 2-(4-BENZYL-PIPERAZIN-1-YL)-BENZOIC ACID ETHYL 4-(2-FORMYLPHENYL)PIPERAZIN-1-CARBOXYLATE 2-[4-(2-FORMYLPHENYL)PIPERAZINO]BENZALDEHYDE 7-[4-(4-FLUOROPHENYL)PIPERAZINO]-3-PHENYL-1-INDANONE RARECHEM AL BE 0461 3-PHENYL-7-(4-PHENYLPIPERAZINO)-1-INDANONE

  • BUTTPARK 33\06-51
  • 2-(4-METHYLPIPERAZIN-1-YL)BENZALDEHYDE
  • 2-(4-METHYLPIPERAZINO)BENZALDEHYDE
  • 2-(4-Methylpiperazino)benzadehyde
  • 2-(4-methyl-1-piperazin-4-iumyl)benzaldehyde
  • Benzaldehyde, 2-(4-methyl-1-piperazinyl)-
  • 2-(4-Methyl-1-piperazinyl)benzaldehyde
  • 85803-62-9
  • Amino Acid Derivatives