bis(3-Methoxyphenyl)aMine
- Product Name
- bis(3-Methoxyphenyl)aMine
- CAS No.
- 92248-06-1
- Chemical Name
- bis(3-Methoxyphenyl)aMine
- Synonyms
- bis(3-Methoxyphenyl)aMine;3-Methoxy-N-(3-methoxyphenyl)aniline;Benzenamine, 3-methoxy-N-(3-methoxyphenyl)-;bis(3-Methoxyphenyl)aMine ISO 9001：2015 REACH
- CBNumber
- CB72610213
- Molecular Formula
- C14H15NO2
- Formula Weight
- 229.27
- MOL File
- 92248-06-1.mol
bis(3-Methoxyphenyl)aMine Property
- Boiling point:
- 175-178 °C(Press: 0.8 Torr)
- Density
- 1.126±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- pka
- 0.14±0.50(Predicted)
N-Bromosuccinimide Price
- Product number
- CHM0391959
- Product name
- BIS-(3-METHOXYPHENYL)AMINE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $505.87
- Updated
- 2021/12/16
- Product number
- 92248061
- Product name
- Bis(3-methoxyphenyl)amine
- Packaging
- 5g
- Price
- $1085.4
- Updated
- 2021/12/16
- Product number
- 92248061
- Product name
- Bis(3-methoxyphenyl)amine
- Packaging
- 10g
- Price
- $1407
- Updated
- 2021/12/16
- Product number
- 92248061
- Product name
- Bis(3-methoxyphenyl)amine
- Packaging
- 25g
- Price
- $2706.8
- Updated
- 2021/12/16
- Product number
- A208352
- Product name
- Bis(3-methoxyphenyl)amine
- Purity
- 95%
- Packaging
- 100mg
- Price
- $21
- Updated
- 2021/12/16
bis(3-Methoxyphenyl)aMine Chemical Properties,Usage,Production
Synthesis
10365-98-7
536-90-3
92248-06-1
General procedure for the synthesis of bis(3-methoxyphenyl)amines from 3-methoxyphenylboronic acid and m-aminoanisole: 1. copper acetate (2.1 mmol) and pyridine (0.25 mL) were added to a vigorously stirred solution of anhydrous dichloromethane (3.5 mL) of 3-methoxyaniline (1 mmol) and 3-methoxyphenylboronic acid (2 mmol) under nitrogen protection. 2. The reaction mixture was stirred at room temperature for 72 hours, during which time the progress of the reaction was monitored by thin layer chromatography (TLC). 3. Upon completion of the reaction, the crude reaction mixture was pre-adsorbed onto silica gel and the target product, bis(3-methoxyphenyl)amine (3c), was subsequently isolated by fast column chromatography. 4. Product yield: 25%; EI-MS m/z: 229 (M+) [Ref: Urgaonkar, S.; Verkade, J.G. J. Org. Chem. 2004, 69, 9135-9142].
References
[1] Patent: WO2007/79593, 2007, A1. Location in patent: Page/Page column 31
bis(3-Methoxyphenyl)aMine Preparation Products And Raw materials
Raw materials
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