ChemicalBook > CAS DataBase List > 2-Methoxy-5-Iodopyridine

2-Methoxy-5-Iodopyridine

Product Name
2-Methoxy-5-Iodopyridine
CAS No.
13472-61-2
Chemical Name
2-Methoxy-5-Iodopyridine
Synonyms
2-Methoxy-5-Iodopyridine;5-lodo-2-methoxypyridine;Pyridine, 5-iodo-2-methoxy-;5-Iodo-2-methoxypyridine>5-Iodo-2-methoxypyridine 98%
CBNumber
CB81033218
Molecular Formula
C6H6INO
Formula Weight
235.02
MOL File
13472-61-2.mol
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2-Methoxy-5-Iodopyridine Property

Boiling point:
237℃
Density 
1.825
refractive index 
1.6060 to 1.6100
Flash point:
97℃
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
form 
Liquid
pka
1.38±0.10(Predicted)
color 
Clear colorless to pale yellow
Sensitive 
Light Sensitive
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Safety

HS Code 
29333990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TCI Chemical
Product number
I0925
Product name
5-Iodo-2-methoxypyridine
Purity
>98.0%(GC)
Packaging
1g
Price
$38
Updated
2025/07/31
TCI Chemical
Product number
I0925
Product name
5-Iodo-2-methoxypyridine
Purity
>98.0%(GC)
Packaging
5g
Price
$119
Updated
2025/07/31
TRC
Product number
I737150
Product name
5-Iodo-2-methoxypyridine
Packaging
100mg
Price
$75
Updated
2021/12/16
AK Scientific
Product number
6238AA
Product name
5-Iodo-2-methoxypyridine
Packaging
1g
Price
$34
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0036532
Product name
5-IODO-2-METHOXYPYRIDINE
Purity
95.00%
Packaging
1G
Price
$642.75
Updated
2021/12/16
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2-Methoxy-5-Iodopyridine Chemical Properties,Usage,Production

Synthesis

13472-85-0

13472-61-2

The general procedure for the synthesis of 5-bromo-2-methoxypyridine from 5-bromo-2-methoxypyridine was as follows: n-butyllithium (1.5 M in hexane solution, 4.98 mL, 7.47 mmol) was slowly added to a solution of isopropylmagnesium chloride (1.61 M in THF, 4.64 mL, 7.47 mmol) in THF (20 mL) under ice bath cooling conditions. The reaction mixture was stirred for 5 min to form a yellow solution after which 5-bromo-2-methoxypyridine (1.405 g, 0.98 mL, 7.10 mmol, 95%) was added. The resulting solution was continued to be stirred at 0 °C for 45 min. Molecular iodine (3.79 g, 14.94 mmol) was then added and the reaction mixture was stirred at 0°C for 30 minutes and then at room temperature for 1 hour. Upon completion of the reaction, the reaction was quenched by the addition of aqueous ammonium chloride (5 mL) and the organic and aqueous phases were separated. The aqueous phase was extracted with ethyl acetate (2 x 75 mL), and the combined organic layers were dried with magnesium sulfate, filtered and concentrated under reduced pressure. The crude product was purified by silica gel column chromatography (ethyl acetate-heptane, 5-80%) to afford the target product 5-iodo-2-methoxypyridine.

References

[1] Synthesis, 2012, vol. 44, # 5, p. 735 - 746
[2] Synthesis (Germany), 2015, vol. 47, # 20, p. 3231 - 3240
[3] Journal of the American Chemical Society, 2015, vol. 137, # 33, p. 10480 - 10483

2-Methoxy-5-Iodopyridine Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-Methoxy-5-Iodopyridine manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD
Product
5-Iodo-2-methoxypyridine 13472-61-2
Price
US $10.00-50.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
g-kg-tons, free sample is available
Release date
2025-06-18
Honest Joy Holdings Limited
Product
5-Iodo-2-methoxypyridine 13472-61-2
Price
US $0.00/KG
Min. Order
1KG
Purity
98.7%
Supply Ability
100 tons
Release date
2022-01-25
Career Henan Chemical Co
Product
2-Methoxy-5-Iodopyridine 13472-61-2
Price
US $1.00/KG
Min. Order
1KG
Purity
99.0%
Supply Ability
100kg
Release date
2020-01-07

13472-61-2, 2-Methoxy-5-IodopyridineRelated Search:

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