3H-Indolium, 1-(2-hydroxyethyl)-2,3,3-trimethyl-, bromide

Product Name: 3H-Indolium, 1-(2-hydroxyethyl)-2,3,3-trimethyl-, bromide
CAS No.: 29636-94-0
Chemical Name: 3H-Indolium, 1-(2-hydroxyethyl)-2,3,3-trimethyl-, bromide
Synonyms: 2-(2,3,3-trimethylindol-1-ium-1-yl)ethanol,bromide;1-(2-Hydroxyethyl)-2,3,3-trimethyl-3H-indol-1-ium bromide;3H-Indolium, 1-(2-hydroxyethyl)-2,3,3-trimethyl-, bromide
CBNumber: CB83215173
Molecular Formula: C13H18BrNO
Formula Weight: 284.19212
MOL File: 29636-94-0.mol

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3H-Indolium, 1-(2-hydroxyethyl)-2,3,3-trimethyl-, bromide Property

storage temp.: Inert atmosphere,Room Temperature
Appearance: Purple to purplish red Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Alichem

Product number: 29636940
Product name: 1-(2-Hydroxyethyl)-2,3,3-trimethyl-3H-indol-1-iumbromide
Packaging: 5g
Price: $178.2
Updated: 2021/12/16

Crysdot

Product number: CD00004929
Product name: 1-(2-Hydroxyethyl)-2,3,3-trimethyl-3H-indol-1-iumbromide
Purity: 97%
Packaging: 10g
Price: $297
Updated: 2021/12/16

Alichem

Product number: 29636940
Product name: 1-(2-Hydroxyethyl)-2,3,3-trimethyl-3H-indol-1-iumbromide
Packaging: 10g
Price: $306
Updated: 2021/12/16

Crysdot

Product number: CD00004929
Product name: 1-(2-Hydroxyethyl)-2,3,3-trimethyl-3H-indol-1-iumbromide
Purity: 97%
Packaging: 25g
Price: $574
Updated: 2021/12/16

Alichem

Product number: 29636940
Product name: 1-(2-Hydroxyethyl)-2,3,3-trimethyl-3H-indol-1-iumbromide
Packaging: 25g
Price: $614.8
Updated: 2021/12/16

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3H-Indolium, 1-(2-hydroxyethyl)-2,3,3-trimethyl-, bromide Chemical Properties,Usage,Production

Synthesis

1640-39-7

540-51-2

29636-94-0

The general procedure for the synthesis of 1-(2-hydroxyethyl)-2,3,3-trimethyl-3H-indole and 2-bromoethanol as raw materials for the synthesis of 1-(2-hydroxyethyl)-2,3,3-trimethyl-3H-indole-1-bromonium was as follows: 3.18 g of 2,3,3-trimethyl-3H-indole and 3.125 g of 2-bromoethanol were dissolved in 30 ml of acetonitrile and transferred to a 100 ml three-necked flask fitted with a condenser. The reaction was slowly heated under nitrogen protection until complete. Upon completion of the reaction, the reaction mixture was slowly cooled to room temperature and the acetonitrile solvent was subsequently removed using a rotary evaporator to give a dark red solid product. To this solid 50 ml of hexane was added and purified by grinding, sonication and filtration. Three grams of the purified product was dissolved in 45 ml of chloroform and recrystallized in a fume hood at 45 °C to give 2.6 g of pink solid product in 87% yield.

References

[1] Synthetic Communications, 2005, vol. 35, # 4, p. 603 - 610
[2] RSC Advances, 2013, vol. 3, # 45, p. 23317 - 23326
[3] Chemical Communications, 2014, vol. 50, # 20, p. 2664 - 2666
[4] Angewandte Chemie - International Edition, 2010, vol. 49, # 43, p. 7968 - 7971
[5] Patent: CN107970448, 2018, A. Location in patent: Paragraph 0021; 0062; 0063

3H-Indolium, 1-(2-hydroxyethyl)-2,3,3-trimethyl-, bromide Preparation Products And Raw materials

Raw materials

Preparation Products

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3H-Indolium, 1-(2-hydroxyethyl)-2,3,3-trimethyl-, bromide Suppliers

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29636-94-0, 3H-Indolium, 1-(2-hydroxyethyl)-2,3,3-trimethyl-, bromideRelated Search:

3H-Indolium, 1-(2-hydroxyethyl)-2,3,3-trimethyl-, bromide

1-(2-Hydroxyethyl)-2,3,3-trimethyl-3H-indol-1-ium bromide

2-(2,3,3-trimethylindol-1-ium-1-yl)ethanol,bromide

29636-94-0

C13H18NOBr