3-AMINO-5-CYANO-BENZOIC ACID METHYL ESTER

Product Name: 3-AMINO-5-CYANO-BENZOIC ACID METHYL ESTER
CAS No.: 199536-01-1
Chemical Name: 3-AMINO-5-CYANO-BENZOIC ACID METHYL ESTER
Synonyms: 3-Amino-5-cyano-benzoic acid me;3-AMINO-5-CYANO-BENZOIC ACID METHYL ESTER;Benzoic acid, 3-amino-5-cyano-, methyl ester;3-AMINO-5-CYANO-BENZOIC ACID METHYL ESTER >98%;3-Amino-5-cyano-benzoic acid methyl ester 95+%
CBNumber: CB9202050
Molecular Formula: C9H8N2O2
Formula Weight: 176.17
MOL File: 199536-01-1.mol

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3-AMINO-5-CYANO-BENZOIC ACID METHYL ESTER Property

Melting point:: 128°C
Boiling point:: 371.5±27.0 °C(Predicted)
Density: 1.26±0.1 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 1?+-.0.10(Predicted)
Appearance: Yellow to brown Solid

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Safety

HS Code: 2916399090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H290May be corrosive to metals

H314Causes severe skin burns and eye damage

H317May cause an allergic skin reaction

Precautionary statements

P234Keep only in original container.

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P271Use only outdoors or in a well-ventilated area.

P272Contaminated work clothing should not be allowed out of the workplace.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P333+P313IF SKIN irritation or rash occurs: Get medical advice/attention.

P390Absorb spillage to prevent material damage.

P405Store locked up.

P406Store in corrosive resistant/… container with a resistant inner liner.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: M878160
Product name: Methyl3-amino-5-cyanobenzoate
Packaging: 50mg
Price: $45
Updated: 2021/12/16

TRC

Product number: M878160
Product name: Methyl3-amino-5-cyanobenzoate
Packaging: 100mg
Price: $90
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4658-1-14
Product name: Methyl 3-amino-5-cyanobenzoate
Purity: 98.0%
Packaging: 250mg
Price: $50
Updated: 2021/12/16

AK Scientific

Product number: 7519BB
Product name: Methyl3-amino-5-cyanobenzoate
Packaging: 1g
Price: $89
Updated: 2021/12/16

Apolloscientific

Product number: OR321011
Product name: 3-Amino-5-cyano-benzoicacidmethylester
Purity: 95+%
Packaging: 5g
Price: $111
Updated: 2021/12/16

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3-AMINO-5-CYANO-BENZOIC ACID METHYL ESTER Chemical Properties,Usage,Production

Synthesis

99066-80-5

199536-01-1

General procedure for the synthesis of methyl 3-amino-5-cyanobenzoate from methyl 3-cyano-5-nitrobenzoate: 10% Pd/C catalyst (0.9 g) was added to a mixed solution of methanol (200 mL) and tetrahydrofuran (100 mL) containing methyl 3-cyano-5-nitrobenzoate (25 mmol). Subsequently, the reaction mixture was stirred at room temperature for 4 hours. Upon completion of the reaction, the catalyst was removed by filtration and the filtrate was concentrated to afford methyl 3-amino-5-cyanobenzoate in 95% yield.

References

[1] Patent: US2009/118292, 2009, A1. Location in patent: Page/Page column 29
[2] Chemistry - A European Journal, 2015, vol. 21, # 52, p. 19231 - 19242
[3] Angewandte Chemie - International Edition, 2004, vol. 43, # 48, p. 6649 - 6652
[4] Patent: WO2011/137587, 2011, A1. Location in patent: Page/Page column 55

3-AMINO-5-CYANO-BENZOIC ACID METHYL ESTER Preparation Products And Raw materials

Raw materials

Preparation Products

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3-AMINO-5-CYANO-BENZOIC ACID METHYL ESTER Suppliers

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199536-01-1