4-BROMO-2-METHOXY-6-METHYLPYRIDINE
- Product Name
- 4-BROMO-2-METHOXY-6-METHYLPYRIDINE
- CAS No.
- 1083169-00-9
- Chemical Name
- 4-BROMO-2-METHOXY-6-METHYLPYRIDINE
- Synonyms
- 4-BROMO-2-METHOXY-6-METHYLPYRIDINE;Pyridine, 4-bromo-2-methoxy-6-methyl-
- CBNumber
- CB92644401
- Molecular Formula
- C7H8BrNO
- Formula Weight
- 202.05
- MOL File
- 1083169-00-9.mol
4-BROMO-2-METHOXY-6-METHYLPYRIDINE Property
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- Appearance
- Colorless to light yellow Liquid
N-Bromosuccinimide Price
- Product number
- B711098
- Product name
- 4-Bromo-2-methoxy-6-methylpyridine
- Packaging
- 500mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- 1674AA
- Product name
- 4-Bromo-2-methoxy-6-methylpyridine
- Packaging
- 5g
- Price
- $2710
- Updated
- 2021/12/16
- Product number
- HCH0365620
- Product name
- 4-BROMO-2-METHOXY-6-METHYLPYRIDINE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $505.79
- Updated
- 2021/12/16
- Product number
- CM170136
- Product name
- 4-bromo-2-methoxy-6-methylpyridine
- Purity
- 95%
- Packaging
- 5g
- Price
- $1122
- Updated
- 2021/12/16
- Product number
- CD11355165
- Product name
- 4-Bromo-2-methoxy-6-methylpyridine
- Purity
- 95+%
- Packaging
- 5g
- Price
- $1188
- Updated
- 2021/12/16
4-BROMO-2-METHOXY-6-METHYLPYRIDINE Chemical Properties,Usage,Production
Synthesis
67-56-1
865156-59-8
1083169-00-9
General procedure for the synthesis of 4-bromo-2-methoxy-6-methylpyridine from methanol and 4-bromo-6-methylpyridin-2-ol: Methanol (54 μL, 1.3 mmol), triphenylphosphine (419 mg, 1.60 mmol), and diisopropyl diazocarboxylate (323 mg, 1.60 mmol) were sequentially added to a solution of 4-bromo-6-methylpyridin-2-ol (200 mg, 1.60 mmol) in THF (4.6 mL) under the protection of nitrogen gas. 1.60 mmol), triphenylphosphine (419 mg, 1.60 mmol) and diisopropyl diazocarboxylate (323 mg, 1.60 mmol). The reaction mixture was stirred at room temperature for 18 hours. After completion of the reaction, it was diluted by adding ethyl acetate and washed (3 times) with 1N NaOH solution. The organic layer was dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure. The crude product was purified by rapid chromatography on silica gel with the eluent ethyl acetate/hexane (5% to 10% gradient) to afford 4-bromo-2-methoxy-6-methylpyridine (65 mg, 0.32 mmol, 30% yield).
References
[1] Patent: WO2016/196644, 2016, A1. Location in patent: Paragraph 675; 676
[2] Patent: WO2018/102452, 2018, A2. Location in patent: Paragraph 659; 660
4-BROMO-2-METHOXY-6-METHYLPYRIDINE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4-BROMO-2-METHOXY-6-METHYLPYRIDINE manufacturers
- Product
- 4-Bromo-2-methoxy-6-methylpyridine 1083169-00-9
- Price
- US $3.00-9.00/KG
- Min. Order
- 0.1KG
- Purity
- 99%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2025-06-26