4,7-dibroMobenzo[1,2-c:4,5-c']bis([1,2,5]thiadiazole)

Product Name: 4,7-dibroMobenzo[1,2-c:4,5-c']bis([1,2,5]thiadiazole)
CAS No.: 165617-59-4
Chemical Name: 4,7-dibroMobenzo[1,2-c:4,5-c']bis([1,2,5]thiadiazole)
Synonyms: M8498;BTT-2Br;4,8-dibromo-;4,5-c']bis[1,2,5]t;4,7-dibroMobenzo[1,2-c;4,8-dibroMobenzo-[1,2-c;4,5-c']bis[1,2,5]thiadiazole;ThBBT,4,8-di(2-thienyl)-benzo[1,2-c;4,7-dibroMobenzo[1,2-c:4,5-c']bis([1,2,5]thiadiazole);4,8-Dibromobenzo[1,2-c:4,5-c']bis([1,2,5]thiadiazole)
CBNumber: CB92645044
Molecular Formula: C6Br2N4S2
Formula Weight: 352.03
MOL File: 165617-59-4.mol

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4,7-dibroMobenzo[1,2-c:4,5-c']bis([1,2,5]thiadiazole) Property

Boiling point:: 469.3±55.0 °C(Predicted)
Density: 3.01±0.1 g/cm3(Predicted)
storage temp.: 2-8°C(protect from light)
InChI: InChI=1S/C6Br2N4S2/c7-1-3-5(11-13-9-3)2(8)6-4(1)10-14-12-6
InChIKey: JIHWVOHZFVWBMK-UHFFFAOYSA-N
SMILES: BrC1C2C(=NSN=2)C(Br)=C2C=1N=S=N2

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

H412Harmful to aquatic life with long lasting effects

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P273Avoid release to the environment.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TCI Chemical

Product number: D4086
Product name: 4,8-Dibromobenzo[1,2-c:4,5-c']bis[[1,2,5]thiadiazole]
Packaging: 1G
Price: $186
Updated: 2025/07/31

TCI Chemical

Product number: D4086
Product name: 4,8-Dibromobenzo[1,2-c:4,5-c']bis[[1,2,5]thiadiazole]
Packaging: 5G
Price: $558
Updated: 2025/07/31

AccelPharmtech

Product number: XP2213
Product name: 4,7-dibroMobenzo[1,2-c:4,5-c']bis([1,2,5]thiadiazole)
Purity: 98.00%
Packaging: 10G
Price: $2260
Updated: 2021/12/16

JR MediChem

Product number: JR6-L6561
Product name: 24d2-Benzo[1,2-c:4,5-c'']bis[1,2,5]thiadiazole,4,8-dibromo-
Purity: 96%
Packaging: 25g
Price: $3980
Updated: 2021/12/16

Ambeed

Product number: A169921
Product name: 4,8-Dibromobenzo[1,2-c:4,5-c']bis([1,2,5]thiadiazole)
Purity: 95%
Packaging: 100mg
Price: $68
Updated: 2021/12/16

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4,7-dibroMobenzo[1,2-c:4,5-c']bis([1,2,5]thiadiazole) Chemical Properties,Usage,Production

Uses

4,7-dibroMobenzo[1,2-c:4,5-c']bis([1,2,5]thiadiazole) is used as an intermediate in optoelectronic and synthetic materials.

Synthesis

141215-32-9

165617-59-4

General procedure for the synthesis of 4,8-dibromobenzo[1,2-c:4,5-c']bis([1,2,5]thiadiazole) from 4,7-dibromobenzo[c][1,2,5]thiadiazole-5,6-diamine: firstly, amine compound (10 g, 30.8 mmol) obtained in step 2 was dissolved in degassed pyridine (300 ml) in an Ar atmosphere protected 1000 ml three-necked flask. Subsequently, N-thienylaniline (9.5 g, 66 mmol) and trimethylmethylsilyl chloride (39.5 g, 363.5 mmol) were added. The reaction mixture was heated to 80 °C and the reaction was stirred at this temperature overnight. After completion of the reaction, the mixture was cooled to room temperature and poured into water (200 ml). The precipitated solid was collected by filtration and washed with a solvent mixture of THF/hexane to give 6 g of crude product. Finally, purification was carried out by silica gel column chromatography (300 g of silica gel, eluent chlorobenzene/hexane, 10:3, v/v) to give 3 g of pure product in 27.6% yield.

References

[1] Angewandte Chemie, 1994, vol. 106, # 19, p. 2030 - 2032
[2] Tetrahedron, 1997, vol. 53, # 29, p. 10169 - 10178
[3] RSC Advances, 2014, vol. 4, # 85, p. 44902 - 44910
[4] Patent: JP2018/111679, 2018, A. Location in patent: Paragraph 0240; 0250; 0251; 0252; 0253
[5] Journal of the American Chemical Society, 2005, vol. 127, # 14, p. 5186 - 5195

4,7-dibroMobenzo[1,2-c:4,5-c']bis([1,2,5]thiadiazole) Preparation Products And Raw materials

Raw materials

Preparation Products

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4,7-dibroMobenzo[1,2-c:4,5-c']bis([1,2,5]thiadiazole) Suppliers

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View Lastest Price from 4,7-dibroMobenzo[1,2-c:4,5-c']bis([1,2,5]thiadiazole) manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD

Product: 4,5-c']bis[1,2,5]thiadiazole 165617-59-4
Price: US $2.00-5.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 100kg
Release date: 2025-06-20

Shaanxi Dideu New Materials Co. Ltd

Product: 4,7-dibroMobenzo[1,2-c:4,5-c']bis([1,2,5]thiadiazole) 165617-59-4
Price: US $0.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 10000KGS
Release date: 2025-05-23

Shaanxi Dideu Medichem Co. Ltd

Product: 4,7-dibroMobenzo[1,2-c:4,5-c']bis([1,2,5]thiadiazole) 165617-59-4
Price: US $0.00-0.00/KG
Min. Order: 1g
Purity: 99%
Supply Ability: 2000tons
Release date: 2019-12-31

165617-59-4, 4,7-dibroMobenzo[1,2-c:4,5-c']bis([1,2,5]thiadiazole)Related Search:

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165617-59-4