Basic information Safety Supplier Related
ChemicalBook >  Product Catalog >  Pharmaceutical intermediates >  Heterocyclic compound >  Pyridine compound >  Chloropyridine >  2-[N,N-BIS(TRIFLUOROMETHANESULFONYL)AMINO]-5-CHLOROPYRIDINE

2-[N,N-BIS(TRIFLUOROMETHANESULFONYL)AMINO]-5-CHLOROPYRIDINE

Basic information Safety Supplier Related

2-[N,N-BIS(TRIFLUOROMETHANESULFONYL)AMINO]-5-CHLOROPYRIDINE Basic information

Product Name:
2-[N,N-BIS(TRIFLUOROMETHANESULFONYL)AMINO]-5-CHLOROPYRIDINE
Synonyms:
  • Comins Reagent, N,N-Bis(trifluoromethylsulfonyl)-5-chloro-2-pyridylamine, 2-[N,N-Bis(trifluoromethylsulfonyl)amino]-5-chloropyridine
  • N-(5-CHLORO-2-PYRIDYL)BIS(TRILFUOROMETHANESULFONIMIDE)
  • N-(5-Chloropyridin-2-yl)-1,1,1-trifluoro-N-(trifluoromethylsulfonyl)methanesulfonamide
  • 2-[N,N-Bis(trifluoromethanesulfonyl)amino]-5-chloropyridine ,98%
  • Comins Triflating Reagent
  • N-(5-Chloro-2-pyridyl)triflimide N-(5-Chloro-2-pyridyl)bis(trifluoromethanesulfonyl)imide Comins Triflating Reagent
  • N-(5-chloropyridin-2-yl)-1,1,1-trifluoro-N-(trifluoroMethane)sulfonylMethanesulfonaMide
  • 2-{Bis[(trifluoromethyl)sulphonyl]amino}-5-chloropyridine
CAS:
145100-51-2
MF:
C7H3ClF6N2O4S2
MW:
392.68
EINECS:
629-110-2
Product Categories:
  • Chloropyridines
  • Halopyridines
Mol File:
145100-51-2.mol
More
Less

2-[N,N-BIS(TRIFLUOROMETHANESULFONYL)AMINO]-5-CHLOROPYRIDINE Chemical Properties

Melting point:
45-47 °C(lit.)
Boiling point:
77-90°C/0.2mmHg
Density 
1.892±0.06 g/cm3(Predicted)
storage temp. 
2-8°C
solubility 
Benzene (Slightly)
form 
Solid
pka
-7.71±0.10(Predicted)
color 
yellow
Water Solubility 
Reacts with water.
Sensitive 
Moisture Sensitive
BRN 
5833971
Stability:
Moisture Sensitive, Unstable in DMSO Solution
InChIKey
TUFGVZMNGTYAQD-UHFFFAOYSA-N
CAS DataBase Reference
145100-51-2(CAS DataBase Reference)
More
Less

Safety Information

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-36
WGK Germany 
3
9
Hazard Note 
Irritant
HazardClass 
AIR SENSITIVE, IRRITANT-HARMFUL, KEEP COLD
HS Code 
29350090

MSDS

More
Less

2-[N,N-BIS(TRIFLUOROMETHANESULFONYL)AMINO]-5-CHLOROPYRIDINE Usage And Synthesis

Chemical Properties

White to pale yellow crystalline solid

Uses

2-[N,N-Bis(trifluoromethylsulfonyl)amino]-5-chloropyridine provides good yields of vinyl triflates from the corresponding ketone enolates or dienolates. It is used in the total synthesis of (-)-porantheridine and the trans decahydroquinoline alkaloid (+)-219A. It is also used as a reactant for Suzuki-Miyaura cross coupling, synthesis of nicotinic acetylcholine receptor-selective ligands, enantioselective desymmetrizing palladium catalyzed carbonylation reactions, synthesis of high affinity niacin receptor GPR109A agonists and in preparation of heteroaromatics.

Uses

Reactant for:
Suzuki-Miyaura cross coupling
Synthesis of nicotinic acetylcholine receptor-selective ligands
Enantioselective desymmetrizing palladium catalyzed carbonylation reactions
Synthesis of high affinity niacin receptor GPR109A agonists
Preparation of heteroaromatics

2-[N,N-BIS(TRIFLUOROMETHANESULFONYL)AMINO]-5-CHLOROPYRIDINESupplier

Beijing Ouhe Technology Co., Ltd Gold
Tel
010-82967028 13552068683
Email
2355560935@qq.com
Jining Huanju Pharmaceutical Co., Ltd. Gold
Tel
0537-2396602 15315373380
Email
1754256732@qq.com
Ningbo Zeyu Chemical Technology Co., Ltd Gold
Tel
15066123231 15066123231
Email
2278736577@qq.com
Wuhan Ruilida Biomedical Technology Co., Ltd. Gold
Tel
18201884268
Email
magean83@163.com
J & K SCIENTIFIC LTD.
Tel
010-82848833 400-666-7788
Email
jkinfo@jkchemical.com