SODIUM PHENOLATE TRIHYDRATE Chemical Properties

Melting point:

61-64 °C(lit.)

storage temp. 

Store below +30°C.

solubility 

soluble in Methanol, Water

form 

solid

Safety Information

Hazard Codes 

C

Risk Statements 

34

Safety Statements 

26-27-28-36/37/39-45

RIDADR 

UN 2905 8/PG 3

WGK Germany 

3

HS Code 

2907 11 00

MSDS

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SODIUM PHENOLATE TRIHYDRATE Usage And Synthesis

Uses

Sodium Phenoxide Trihydrate, is used in the synthesis of trialkylphosphonium salts as replacements for easily oxidizable trialkylphosphines. Also used in the aminocarbonylation of aryl chlorides at atmospheric pressure.

Purification Methods

The ground powder is washed with Et2O, then heated at 60o/1mm for 12 to 24hours to remove any free phenol and solvent. [Kornblum & Lurie J Am Chem Soc 81 2710 1959, Beilstein 6 I 718.]

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