(3-BROMOBENZYL)DIMETHYLAMINE Chemical Properties

Melting point:

139-141 °C

Boiling point:

105-108 °C(Press: 9.8 Torr)

Density 

1.5 g/cm3(Temp: 19 °C)

storage temp. 

2-8°C(protect from light)

pka

8.71±0.28(Predicted)

Appearance

Colorless to light yellow Liquid

Safety Information

Hazard Codes 

Xi

HazardClass 

IRRITANT

HS Code 

2921490090

(3-BROMOBENZYL)DIMETHYLAMINE Usage And Synthesis

Synthesis

The general procedure for the synthesis of (3-bromophenyl)dimethylamine from 3-bromobenzyl bromide was as follows:(i) Dimethylamine (51.4 g, 1.14 mol) was reacted with 3-bromobenzyl bromide (95 g, 0.38 mol) in benzene at 5 °C. Upon completion of the reaction, the reaction mixture was acidified with hydrochloric acid and subsequently extracted with 3N hydrochloric acid aqueous solution. The aqueous extract was adjusted to alkaline with aqueous potassium hydroxide and the oily product was isolated by distillation to afford 3-bromo-N,N-dimethylbenzylamine (65 g, 80% yield) with a boiling point of 118°C/20 mmHg.

References

[1] Patent: US4496567, 1985, A

(3-BROMOBENZYL)DIMETHYLAMINE(4885-18-1)Related Product Information

• BROMOHEXINE
• 6-BROMO-3-METHYLQUINAZOLIN-4(3H)-ONE
• 4-(3-BROMOBENZOYL) MORPHOLINE
• Bromhexine hydrochloride
• (3-bromophenylcarbonyl)piperidine
• Arbidol hydrochloride
• (4-BROMOBENZYL)DIMETHYLAMINE,(4-Bromophenyl)-N,N-dimethylmethylamine, (4-Bromobenzyl)dimethylamine
• 6-bromo-3-phenyl-2,4(1H,3H)-quinazolinedione
• 2-BENZYL-5-BROMOISOINDOLINE-1,3-DIONE
• 6-bromo-3-ethyl-2,4(1H,3H)-quinazolinedione
• (2-BROMOBENZYL)DIMETHYLAMINE
• 10-BROMO-3-(4-CHLOROPHENYL)SPIRO[1,3-THIAZOLIDINE-2,3'-INDOLINE]-4,7-DIONE
• 4,5,6,7-TETRABROMO-2-(OXIRAN-2-YLMETHYL)ISOINDOLINE-1,3-DIONE
• BROMOCRESOL ORANGE
• AURORA 19777
• 6-BROMO-2-MERCAPTO-3-PHENYLQUINAZOLIN-4(3H)-ONE
• 6-CHLORO-1-[(3-BROMO-4-METHOXYPHENYL)METHYL]-3-METHYL-2,4(1H,3H)-PYRIMIDINEDIONE
• N,N'-(methylenedi-p-phenylene)bis[3,4,5,6,-tetrabromophthalimide]