ChemicalBook > Product Catalog > Organic Chemistry > Organic fluorine compound > Series fluorobenzyl alcohol > 4-Chloro-2-fluorobenzyl alcohol
4-Chloro-2-fluorobenzyl alcohol
4-Chloro-2-fluorobenzyl alcohol Basic information
- Product Name:
- 4-Chloro-2-fluorobenzyl alcohol
- Synonyms:
-
- RARECHEM AL BD 0387
- 4-CHLORO-2-FLUOROBENZYL ALCOHOL
- (4-chloro-2-fluorophenyl)Methanol
- Benzenemethanol, 4-chloro-2-fluoro-
- 4-Chloro-2-fluorobenzyl alcohol ISO 9001:2015 REACH
- (3,3'-DITHIOBISHYDROCINNAMIC ACID
- CAS:
- 56456-49-6
- MF:
- C7H6ClFO
- MW:
- 160.57
- EINECS:
- 671-284-7
- Product Categories:
-
- Alcohols
- Chlorine Compounds
- Benzhydrols, Benzyl & Special Alcohols
- Fluorine Compounds
- Mol File:
- 56456-49-6.mol
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4-Chloro-2-fluorobenzyl alcohol Chemical Properties
- Boiling point:
- 227.6±25.0 °C(Predicted)
- Density
- 1.344±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 13.68±0.10(Predicted)
- CAS DataBase Reference
- 56456-49-6(CAS DataBase Reference)
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Safety Information
- Hazard Codes
- Xi
- Risk Statements
- 36/37/38
- Safety Statements
- 26-36/37/39
- HazardClass
- IRRITANT
- HS Code
- 2906290090
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4-Chloro-2-fluorobenzyl alcohol Usage And Synthesis
Synthesis
A solution of 4-chloro-2-fluorobenzoic acid (300mg) in THF (15m1) was added at 0CLiAIH4 (130mg). The suspension was stirred at 0℃ for 16h. The reaction mixture was diluted with EA and aq. A solution of potassium sodium tartrate was stirred for lh at rt. The layers were separated, and the org. phasel was further washed with water. The combined org. layers were dried over MgSO4, filtrated off and evaporated in vacuo. The crude was purified by CC (Buechi Sepacore, 5g cartridge, solvent A: DCM, solvent B: 3N ammonia in MeOH, gradient in %B: 0 to 5, flow rate: 6.0 mI/mm) to afford 224mg of colourless oil 4-Chloro-2-fluorobenzyl alcohol. LCMS: (A) tR = 0.68 mm; [M+H]: not visible.
4-Chloro-2-fluorobenzyl alcoholSupplier
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4-Chloro-2-fluorobenzyl alcohol(56456-49-6)Related Product Information
- 4-Fluorobenzyl chloride
- alpha-Chloro-o-fluorotoluene
- 1,2-Difluorobenzene
- Benzyl chloroformate
- 4-Nitrobenzyl alcohol
- MCPA SODIUM
- 1,2-Dichloro-4-(chloromethyl)benzene
- Benzyl alcohol
- Transfluthrin
- 4-Fluorobenzaldehyde
- 3-Fluorobenzyl alcohol
- 4-Chlorobenzyl chloride
- 3-Chlorobenzyl chloride
- Ethyl acetate
- 2-Chlorobenzyl chloride
- Florfenicol
- Difluorochloromethane
- 4-Chloro-2-fluoro-5-sulfamylbenzoic acid