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fenetylline hydrochloride

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fenetylline hydrochloride Basic information

Product Name:
fenetylline hydrochloride
Synonyms:
  • fenetylline hydrochloride
  • Fenethylline
  • Fenetylline
  • Fenethylline hydrochloride
  • 1H-Purine-2,6-dione, 3,7-dihydro-1,3-dimethyl-7-[2-[(1-methyl-2-phenylethyl)amino]ethyl]-, monohydrochloride
  • 7-(Phenyl-isopropyl-amino-aethyl)-theophyllin-hydrochlorid
  • 7-[2-(1-Methyl-2-phenylethylamino)ethyl]theophylline hydrochloride
  • 7-[2-[(.alpha.-Methylphenethyl)amino]ethyl]theophylline hydrochloride
CAS:
1892-80-4
MF:
C18H24ClN5O2
MW:
377.86846
EINECS:
217-580-8
Product Categories:
  • Amines
  • Aromatics
  • Bases & Related Reagents
  • Intermediates & Fine Chemicals
  • Nucleotides
  • Pharmaceuticals
Mol File:
1892-80-4.mol
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fenetylline hydrochloride Chemical Properties

Melting point:
227-229°; mp 237-239°
solubility 
DMF: 0.3 mg/ml; DMSO: 0.5 mg/ml; PBS (pH 7.2): 10 mg/ml
form 
A crystalline solid
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Safety Information

Toxicity
LD50 oral in rat: 100mg/kg
DEA Controlled Substances
CSCN: 1503
CAS SCH: I
NARC: N
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fenetylline hydrochloride Usage And Synthesis

Originator

Captagon,Homburg,W. Germany,1961

Uses

CNS stimulant. Controlled substance.

Manufacturing Process

1 mol of 7-(β-chloroethyl)-theophylline and 2? mols of α-methyl-β-phenyl ethylamine are heated for 6 hours in an oil bath, if necessary with addition of alcohol or toluene. The reaction mixture is diluted with alcohol and acidified with alcoholic hydrochloric acid. The crystalline mass formed is filtered with suction and extracted by boiling with alcohol. A product having a melting point of 237°C to 239°C is formed. With prolonged extraction by boiling with alcohol, the melting point of the mass falls, preferably due to a change in modification, to 227°C to 229°C. However, analysis shows that both products are the pure condensation product.
Instead of the chloroethyl theophylline, it is also possible to use the corresponding bromine derivative. It was found that in this way the process is facilitated and the yield is improved

Therapeutic Function

Central stimulant

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fenetylline hydrochloride(1892-80-4)Related Product Information