methyl hydrazonothiocarbamate
methyl hydrazonothiocarbamate Basic information
- Product Name:
- methyl hydrazonothiocarbamate
- Synonyms:
-
- methyl hydrazonothiocarbamate
- S-Methylisothiosemicarbazide
- Hydrazinecarboximidothioic acid, methyl ester
- methyl (E)-carbamohydrazonothioate
- 1-Amino-2-methylisothiourea
- CAS:
- 44387-06-6
- MF:
- C2H7N3S
- MW:
- 105.16
- EINECS:
- 604-604-1
- Mol File:
- 44387-06-6.mol
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methyl hydrazonothiocarbamate Chemical Properties
- Melting point:
- 136-137 °C
- Boiling point:
- 166.2±23.0 °C(Predicted)
- Density
- 1.38±0.1 g/cm3(Predicted)
- pka
- 6.37±0.50(Predicted)
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methyl hydrazonothiocarbamate Usage And Synthesis
Uses
Methyl hydrazonothiocarbamate is used for synthesis of substituted 1,2,4-triazines, tetrazoles, and guanylhydrazones.
Preparation
HI salt of methyl hydrazonothiocarbamate is prepared by refluxing thiosemicarbazide and methyl iodide in absolute ethanol for 45 min. Crystallized upon cooling the reaction mixture to give 90% yield. Recrystallized from absolute ethanol.
Precautions
Use in a fume hood.
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methyl hydrazonothiocarbamate(44387-06-6)Related Product Information
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- S-METHYL ISOTHIOSEMICARBAZIDE HYDROIODIDE
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- ISOMETHIOZIN
- methyl hydrazonothiocarbamate
- 1-(4,5-DIHYDRO-1,3-THIAZOL-2-YL)-3-METHYL-1H-PYRAZOLE-4,5-DIONE 4-(N-[3-(TRIFLUOROMETHYL)PHENYL]HYDRAZONE)
- 2-HYDRAZINO-4,5-DIHYDRO-1,3-THIAZOLE
- ETHYL 2-[(4,6-DIAMINO-5-OXO-4,5-DIHYDRO-1,2,4-TRIAZIN-3-YL)THIO]ACETATE
- 1-[[(4-METHYLBENZYL)SULFANYL](METHYLIMINO)METHYL]-3-OXOTETRAHYDRO-1H-PYRAZOL-1-IUM CHLORIDE
- 4-AMINO-3-[(4-CHLOROBENZYL)THIO]-6-METHYL-4,5-DIHYDRO-1,2,4-TRIAZIN-5-ONE
- 1-[[(2-CHLOROBENZYL)SULFANYL](METHYLIMINO)METHYL]-3-OXOTETRAHYDRO-1H-PYRAZOL-1-IUM CHLORIDE
- 1-(4,5-DIHYDRO-1,3-THIAZOL-2-YL)-3-METHYL-1H-PYRAZOLE-4,5-DIONE 4-(N-PHENYLHYDRAZONE)
- 1-[[(3-CHLOROBENZYL)SULFANYL](METHYLIMINO)METHYL]-3-OXOTETRAHYDRO-1H-PYRAZOL-1-IUM CHLORIDE
- BUTTPARK 15\07-63
- 2-IMINO-5,5-DIOXO-TETRAHYDRO-5LAMBDA6-THIENO[3,4-D]THIAZOL-3-YLAMINE
- 4-AMINO-6-[4-(DIMETHYLAMINO)BENZYL]-3-(METHYLTHIO)-4,5-DIHYDRO-1,2,4-TRIAZIN-5-ONE