Basic information Safety Supplier Related

methyl hydrazonothiocarbamate

Basic information Safety Supplier Related

methyl hydrazonothiocarbamate Basic information

Product Name:
methyl hydrazonothiocarbamate
Synonyms:
  • methyl hydrazonothiocarbamate
  • S-Methylisothiosemicarbazide
  • Hydrazinecarboximidothioic acid, methyl ester
  • methyl (E)-carbamohydrazonothioate
  • 1-Amino-2-methylisothiourea
CAS:
44387-06-6
MF:
C2H7N3S
MW:
105.16
EINECS:
604-604-1
Mol File:
44387-06-6.mol
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methyl hydrazonothiocarbamate Chemical Properties

Melting point:
136-137 °C
Boiling point:
166.2±23.0 °C(Predicted)
Density 
1.38±0.1 g/cm3(Predicted)
pka
6.37±0.50(Predicted)
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methyl hydrazonothiocarbamate Usage And Synthesis

Uses

Methyl hydrazonothiocarbamate is used for synthesis of substituted 1,2,4-triazines, tetrazoles, and guanylhydrazones.

Preparation

HI salt of methyl hydrazonothiocarbamate is prepared by refluxing thiosemicarbazide and methyl iodide in absolute ethanol for 45 min. Crystallized upon cooling the reaction mixture to give 90% yield. Recrystallized from absolute ethanol.

Precautions

Use in a fume hood.

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