4-Methyl-3-nitrobenzoyl chloride Chemical Properties

Melting point:

20-21 °C(lit.)

Boiling point:

185 °C36 mm Hg(lit.)

Density 

1.37 g/mL at 25 °C(lit.)

refractive index 

n20/D 1.581(lit.)

Flash point:

>230 °F

CAS DataBase Reference

10397-30-5(CAS DataBase Reference)

NIST Chemistry Reference

4-Methyl-3-nitrobenzoyl chloride(10397-30-5)

Safety Information

Hazard Codes 

C

Risk Statements 

34

Safety Statements 

26-27-36/37/39-45

RIDADR 

UN 3265 8/PG 2

WGK Germany 

3

HS Code 

2916399090

MSDS

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4-Methyl-3-nitrobenzoyl chloride Usage And Synthesis

Uses

4-Methyl-3-nitrobenzoyl chloride was used in the synthesis of 4-amino-1,5-naphthalenedisulphonate acid monosodium salt, an intermediate employed in the synthesis of modified suramin molecule.
It may be used in the synthesis of the following:

• benzophenone derivative
• substituted 3-amino-4-methyl-N-phenylbenzamide
• retroamide
• 4-methyl-3-nitro-N-phenylbenzamide

General Description

4-Methyl-3-nitrobenzoyl chloride is a benzoyl chloride derivative. It has been reported to be synthesized from 4-methyl-3-nitrobenzoic acid.

Purification Methods

Recrystallise the acid from EtOH. The S-benzylisothiuronium salt has m 167-168o (EtOH). The acid chloride [10397-30-5] has m 20-21o, b 185o/36mm, and the methyl ester [7356-11-8] crystallises as pale yellow needles from MeOH with m 51o. [Beilstein 9 H 502, 9 II 334, 9 III 2359.]

4-Methyl-3-nitrobenzoyl chloride(10397-30-5)Related Product Information

• o-Toluoyl chloride
• Benzoyl chloride
• Methyl acetate
• 4-Fluorobenzoyl chloride
• Kresoxim-methyl
• Methyl salicylate
• Thiophanate-methyl
• p-Toluoyl chloride
• Pirimiphos-methyl
• 4-Methoxybenzoyl chloride
• 4-(Chloromethyl)benzoyl chloride
• alpha,alpha,alpha-Trifluoro-o-toluoyl chloride
• 4-Chlorobenzoyl chloride
• Tribenuron methyl
• METSULFURON METHYL
• Methyl
• 2-Nitrobenzoyl chloride
• NITROGEN DIOXIDE