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1H,1H,2H-Perfluoro-1-decene

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1H,1H,2H-Perfluoro-1-decene Basic information

Product Name:
1H,1H,2H-Perfluoro-1-decene
Synonyms:
  • 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-Heptadecafluoro-1-decene,99%
  • (Perfluoroct-1-yl)ethylene, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-Heptadecafluorodec-1-ene
  • 1H,1H,2H-Heptadecafluorodec-1-ene 97%
  • 1H,1H,2H-Perfluoro-1-decene 99%
  • 1,1,2-Trihydroperfluoro-1-decene
  • 1H,1H,2H-PERFLUORODEC-1-ENE
  • 1H,1H,2H-PERFLUORO-1-DECENE
  • 1H,1H,2H-HEPTADECAFLUORO-1-DECENE
CAS:
21652-58-4
MF:
C10H3F17
MW:
446.1
EINECS:
244-503-5
Product Categories:
  • Fluorous Compounds
  • Synthetic Organic Chemistry
  • Fluorous Chemistry
Mol File:
21652-58-4.mol
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1H,1H,2H-Perfluoro-1-decene Chemical Properties

Boiling point:
146-147 °C
Density 
1.677 g/mL at 25 °C (lit.)
refractive index 
n20/D 1.301(lit.)
Flash point:
>230 °F
storage temp. 
Refrigerator
solubility 
Chloroform (Sparingly), Methanol (Slightly)
form 
Oil
color 
Colourless
Specific Gravity
1.677
Water Solubility 
Insoluble in water.
BRN 
2066558
InChIKey
NKAMGQZDVMQEJL-UHFFFAOYSA-N
CAS DataBase Reference
21652-58-4(CAS DataBase Reference)
NIST Chemistry Reference
1h,1h,2h-Perfluoro-1-decene(21652-58-4)
EPA Substance Registry System
Perfluorooctyl Ethylene (21652-58-4)
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Safety Information

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-36
RIDADR 
1993
WGK Germany 
3
Hazard Note 
Harmful
TSCA 
T
HazardClass 
3.2
PackingGroup 
III
HS Code 
29033990

MSDS

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1H,1H,2H-Perfluoro-1-decene Usage And Synthesis

Chemical Properties

clear colorless liquid

Uses

1H,1H,2H-Perfluoro-1-decene is useful in the chemical process of making an electrolyte-phobic surface for next generation nanostructured battery electrodes.

Synthesis

 98% sodium hydroxide 108.535 mmol and methanol 38.74g were introduced into a 200mL eggplant flask which was equipped with a Dimroth condenser, the mixture was stirred at 50 °C until sodium hydroxide was dissolved. Sodium hydroxide amount to 1 liter of methanol in this case was 2.17 mol. After the sodium hydroxide had dissolved 1H, 1H, 2H, 2H-1-iodoperfluorodecane 104.996mmol was charged and further stirred for 2 hours at 50 °C. Heating and stirring were stopped, the obtained two-layer solution which became slightly pale brown turbid was separated after standing, and 45.81g lower layer was collected as 1H,1H,2H-perfluorodecene. As a result of analysis by gas chromatography, purity was 98.59%. The weight of the separated methanol layer was 56.10g.

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