1H,1H,2H-Perfluoro-1-decene
1H,1H,2H-Perfluoro-1-decene Basic information
- Product Name:
- 1H,1H,2H-Perfluoro-1-decene
- Synonyms:
-
- 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-Heptadecafluoro-1-decene,99%
- (Perfluoroct-1-yl)ethylene, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-Heptadecafluorodec-1-ene
- 1H,1H,2H-Heptadecafluorodec-1-ene 97%
- 1H,1H,2H-Perfluoro-1-decene 99%
- 1,1,2-Trihydroperfluoro-1-decene
- 1H,1H,2H-PERFLUORODEC-1-ENE
- 1H,1H,2H-PERFLUORO-1-DECENE
- 1H,1H,2H-HEPTADECAFLUORO-1-DECENE
- CAS:
- 21652-58-4
- MF:
- C10H3F17
- MW:
- 446.1
- EINECS:
- 244-503-5
- Product Categories:
-
- Fluorous Compounds
- Synthetic Organic Chemistry
- Fluorous Chemistry
- Mol File:
- 21652-58-4.mol
1H,1H,2H-Perfluoro-1-decene Chemical Properties
- Boiling point:
- 146-147 °C
- Density
- 1.677 g/mL at 25 °C (lit.)
- refractive index
- n20/D 1.301(lit.)
- Flash point:
- >230 °F
- storage temp.
- Refrigerator
- solubility
- Chloroform (Sparingly), Methanol (Slightly)
- form
- Oil
- color
- Colourless
- Specific Gravity
- 1.677
- Water Solubility
- Insoluble in water.
- BRN
- 2066558
- InChIKey
- NKAMGQZDVMQEJL-UHFFFAOYSA-N
- CAS DataBase Reference
- 21652-58-4(CAS DataBase Reference)
- NIST Chemistry Reference
- 1h,1h,2h-Perfluoro-1-decene(21652-58-4)
- EPA Substance Registry System
- Perfluorooctyl Ethylene (21652-58-4)
MSDS
- Language:English Provider:1H,1H,2H-Perfluoro-1-decene
- Language:English Provider:SigmaAldrich
- Language:English Provider:ACROS
- Language:English Provider:ALFA
1H,1H,2H-Perfluoro-1-decene Usage And Synthesis
Chemical Properties
clear colorless liquid
Uses
1H,1H,2H-Perfluoro-1-decene is useful in the chemical process of making an electrolyte-phobic surface for next generation nanostructured battery electrodes.
Synthesis
98% sodium hydroxide 108.535 mmol and methanol 38.74g were introduced into a 200mL eggplant flask which was equipped with a Dimroth condenser, the mixture was stirred at 50 °C until sodium hydroxide was dissolved. Sodium hydroxide amount to 1 liter of methanol in this case was 2.17 mol. After the sodium hydroxide had dissolved 1H, 1H, 2H, 2H-1-iodoperfluorodecane 104.996mmol was charged and further stirred for 2 hours at 50 °C. Heating and stirring were stopped, the obtained two-layer solution which became slightly pale brown turbid was separated after standing, and 45.81g lower layer was collected as 1H,1H,2H-perfluorodecene. As a result of analysis by gas chromatography, purity was 98.59%. The weight of the separated methanol layer was 56.10g.
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