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1-Iodoheptane

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1-Iodoheptane Basic information

Product Name:
1-Iodoheptane
Synonyms:
  • I-Iodoheptane
  • 1-Iodoheptane99%
  • 1-Iodoheptane,98%
  • 1-Iodoheptane (stabilized with Copper chip)
  • 1-Iodoheptane, 98%, stab. with copper
  • 1-Jodheptan
  • 1-IODOHEPTANE1-IODOHEPTANE1-IODOHEPTANE1-IODOHEPTANE
  • Iodoheptane
CAS:
4282-40-0
MF:
C7H15I
MW:
226.1
EINECS:
224-285-8
Product Categories:
  • Iodine Compounds
Mol File:
4282-40-0.mol
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1-Iodoheptane Chemical Properties

Melting point:
-48 °C (lit.)
Boiling point:
204 °C (lit.)
Density 
1.379 g/mL at 25 °C (lit.)
refractive index 
n20/D 1.490(lit.)
Flash point:
174 °F
storage temp. 
Keep in dark place,Sealed in dry,Room Temperature
solubility 
benzene: miscible(lit.)
form 
clear liquid
color 
Colorless to Brown
Specific Gravity
1.379
Water Solubility 
immiscible
Sensitive 
Light Sensitive
BRN 
1697161
Dielectric constant
4.9(22℃)
CAS DataBase Reference
4282-40-0(CAS DataBase Reference)
NIST Chemistry Reference
1-Iodoheptane(4282-40-0)
EPA Substance Registry System
Heptane, 1-iodo- (4282-40-0)
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Safety Information

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-36-37/39
WGK Germany 
3
RTECS 
MJ1050000
8
Hazard Note 
Irritant
TSCA 
Yes
HS Code 
29033080

MSDS

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1-Iodoheptane Usage And Synthesis

Chemical Properties

It is a clear, colorless to pale yellow-orange liquid. It is not soluble in water but dissolves readily in ethanol, ether, acetone, and chloroform. If exposed to light or stored for a long time, it may become discolored.

Uses

1-Iodoheptane is used in the functionalization of symmetrical star-shaped molecules with carborane clusters.

Synthesis

The Synthesis of 1-iodoheptane is as follows:
Firstly, catechol reacts with phosphorus trichloride to produce o-phenylene phosphorous acid chloride, and then the produced compound reacts with heptanol to obtain colorless oily phosphite. Second, take 50.9g (0.20mol) of the above phosphite and 50.8g (0.20mol) of iodine into 500ml of dichloromethane. After that, stir at room temperature for 1h. Finally, use 10% sodium thiosulfate solution to wash away the unreacted iodine that may exist, then wash with 5% NaOH solution, 5% NaHCO3 solution, and saturated NaCl solution in turn, separate the organic phase, evaporate the solvent, and depressurize Distill and collect fractions at 96-104°C (5.33-6.4kPa) to obtain 39g 1-Iodoheptane with a yield of 86%.

1-Iodoheptane Preparation Products And Raw materials

Raw materials

1-IodoheptaneSupplier

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