1-Iodoheptane
1-Iodoheptane Basic information
- Product Name:
- 1-Iodoheptane
- Synonyms:
-
- I-Iodoheptane
- 1-Iodoheptane99%
- 1-Iodoheptane,98%
- 1-Iodoheptane (stabilized with Copper chip)
- 1-Iodoheptane, 98%, stab. with copper
- 1-Jodheptan
- 1-IODOHEPTANE1-IODOHEPTANE1-IODOHEPTANE1-IODOHEPTANE
- Iodoheptane
- CAS:
- 4282-40-0
- MF:
- C7H15I
- MW:
- 226.1
- EINECS:
- 224-285-8
- Product Categories:
-
- Iodine Compounds
- Mol File:
- 4282-40-0.mol
1-Iodoheptane Chemical Properties
- Melting point:
- -48 °C (lit.)
- Boiling point:
- 204 °C (lit.)
- Density
- 1.379 g/mL at 25 °C (lit.)
- refractive index
- n20/D 1.490(lit.)
- Flash point:
- 174 °F
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- solubility
- benzene: miscible(lit.)
- form
- clear liquid
- color
- Colorless to Brown
- Specific Gravity
- 1.379
- Water Solubility
- immiscible
- Sensitive
- Light Sensitive
- BRN
- 1697161
- Dielectric constant
- 4.9(22℃)
- CAS DataBase Reference
- 4282-40-0(CAS DataBase Reference)
- NIST Chemistry Reference
- 1-Iodoheptane(4282-40-0)
- EPA Substance Registry System
- Heptane, 1-iodo- (4282-40-0)
Safety Information
- Hazard Codes
- Xi
- Risk Statements
- 36/37/38
- Safety Statements
- 26-36-37/39
- WGK Germany
- 3
- RTECS
- MJ1050000
- F
- 8
- Hazard Note
- Irritant
- TSCA
- Yes
- HS Code
- 29033080
MSDS
- Language:English Provider:1-Iodoheptane
- Language:English Provider:SigmaAldrich
- Language:English Provider:ACROS
- Language:English Provider:ALFA
1-Iodoheptane Usage And Synthesis
Chemical Properties
It is a clear, colorless to pale yellow-orange liquid. It is not soluble in water but dissolves readily in ethanol, ether, acetone, and chloroform. If exposed to light or stored for a long time, it may become discolored.
Uses
1-Iodoheptane is used in the functionalization of symmetrical star-shaped molecules with carborane clusters.
Synthesis
The Synthesis of 1-iodoheptane is as follows:
Firstly, catechol reacts with phosphorus trichloride to produce o-phenylene phosphorous acid chloride, and then the produced compound reacts with heptanol to obtain colorless oily phosphite. Second, take 50.9g (0.20mol) of the above phosphite and 50.8g (0.20mol) of iodine into 500ml of dichloromethane. After that, stir at room temperature for 1h. Finally, use 10% sodium thiosulfate solution to wash away the unreacted iodine that may exist, then wash with 5% NaOH solution, 5% NaHCO3 solution, and saturated NaCl solution in turn, separate the organic phase, evaporate the solvent, and depressurize Distill and collect fractions at 96-104°C (5.33-6.4kPa) to obtain 39g 1-Iodoheptane with a yield of 86%.
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1-Iodoheptane(4282-40-0)Related Product Information
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