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2-Chlorobenzamide

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2-Chlorobenzamide Basic information

Product Name:
2-Chlorobenzamide
Synonyms:
  • Benzamide, o-chloro
  • 2-Chlorobenzamide,98%
  • o-chloro-benzamid
  • TIMTEC-BB SBB004023
  • O-CHLORO-BENZAMIDE
  • 2-chloro-benzamid
  • 2-CHLOROBENZAMIDE
  • 2-Chlorbenzamid
CAS:
609-66-5
MF:
C7H6ClNO
MW:
155.58
EINECS:
210-195-6
Product Categories:
  • API Intermediate
  • Aromatic Carboxylic Acids, Amides, Anilides, Anhydrides & Salts
  • Anilines, Amides & Amines
  • Chlorine Compounds
  • Amides
  • Carbonyl Compounds
  • Organic Building Blocks
Mol File:
609-66-5.mol
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2-Chlorobenzamide Chemical Properties

Melting point:
142-144 °C(lit.)
Boiling point:
275.0±23.0 °C(Predicted)
Density 
1.2187 (rough estimate)
refractive index 
1.5618 (estimate)
storage temp. 
Sealed in dry,Room Temperature
form 
powder to crystal
pka
15.36±0.50(Predicted)
color 
White to Almost white
BRN 
508510
CAS DataBase Reference
609-66-5(CAS DataBase Reference)
EPA Substance Registry System
2-Chlorobenzamide (609-66-5)
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Safety Information

Hazard Codes 
Xn
Risk Statements 
22-36/37/38-20/22
Safety Statements 
36-37/39-26
WGK Germany 
1
RTECS 
CV2443737
TSCA 
Yes
HazardClass 
IRRITANT
HS Code 
2924297099

MSDS

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2-Chlorobenzamide Usage And Synthesis

Chemical Properties

The substance is an almost white crystalline powder that can be dissolved in solvents such as benzene and toluene.

Uses

2-Chlorobenzamide is used to synthesize chlortetracycline and o-chlorobenzoyl isocyanate, which is an intermediate in chlortetracycline synthesis.

General Description

2-Chlorobenzamide is the major degradation product of CCU (1-(2-chlorobenzoyl)-3-(4-chlorophenyl) urea), a new insect growth regulator. It undergoes room temperature Pd-mediated hydrodehalogenations with KF and polymethylhydrosiloxane (PMHS) to yield benzamide. t undergoes reduction with NaBH4 in diglyme at 162°C to yield 2-chlorobenzonitrile.

Synthesis

Prepared by reacting o-chlorobenzoyl chloride with ammonia.

2-Chlorobenzamide Preparation Products And Raw materials

Raw materials

Preparation Products

2-ChlorobenzamideSupplier

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