DIETHYL ISOPHTHALATE
DIETHYL ISOPHTHALATE Basic information
- Product Name:
- DIETHYL ISOPHTHALATE
- Synonyms:
-
- RARECHEM AL BI 0071
- 1,3-Benzenedicarboxylicacid,diethylester
- Diethyl isophthlate
- Diethylm-phthalate
- Isophthalic acid, diethyl ester
- isophthalicacid,diethylester
- isophthalicaciddiethylester
- DIETHYL ISOPHTHALATE
- CAS:
- 636-53-3
- MF:
- C12H14O4
- MW:
- 222.24
- EINECS:
- 211-260-1
- Mol File:
- 636-53-3.mol
DIETHYL ISOPHTHALATE Chemical Properties
- Melting point:
- 11.5°C
- Boiling point:
- 302°C (estimate)
- Density
- 1.1239
- refractive index
- 1.5080 (estimate)
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- Colorless to light yellow Liquid
- EPA Substance Registry System
- Diethyl isophthalate (636-53-3)
Safety Information
- Hazardous Substances Data
- 636-53-3(Hazardous Substances Data)
DIETHYL ISOPHTHALATE Usage And Synthesis
Synthesis
121-91-5
109-63-7
636-53-3
In a 50 mL two-necked round-bottomed flask fitted with a magnetic stirrer, fitted with a reflux condenser and connected to a calcium chloride drying tube, isophthalic acid (1 g, 8.1 mmol) was suspended in boron trifluoride ethyl ether complex (10 mL). The reaction mixture was stirred and heated at 120 °C overnight, during which the milky white mixture gradually changed to a brown solution. The progress of the reaction was monitored by thin-layer chromatography (unfolding agent: hexane/ethyl acetate, 3:1, v/v) to confirm that the reaction was complete. After the reaction mixture was cooled, it was diluted with deionized water (25 mL) and subsequently extracted with ethyl acetate (3 x 10 mL). The organic phases were combined and washed with saturated sodium bicarbonate solution until no bubbles were produced. The organic layer was dried over anhydrous sodium sulfate and concentrated under reduced pressure to give 1.11 g of crude product in 92% yield.
References
[1] Bulletin of the Chemical Society of Ethiopia, 2018, vol. 32, # 2, p. 387 - 392
DIETHYL ISOPHTHALATE Preparation Products And Raw materials
Preparation Products
Raw materials
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DIETHYL ISOPHTHALATE(636-53-3)Related Product Information
- Mono-methyl isophthalate
- Dimethyl isophthalate
- Sodium dimethyl 5-sulphonatoisophthalate
- Diphenyl isophthalate
- TRIISONONYL TRIMELLITATE
- TRI-ISODECYL TRIMELLITATE
- TRIOCTYL TRIMELLITATE
- Triallyl trimellitate
- Trioctyl trimellitate
- Diethyl 5-nitroisophthalate
- sodium bis(2-hydroxyethyl) 5-sulphonatoisophthalate
- DIALLYL ISOPHTHALATE
- TRIMELLITIC ACID TRI-N-BUTYL ESTER
- NITROTHAL-ISOPROPYL
- DIETHYL 5-(HYDROXYMETHYL)ISOPHTHALATE
- Isophthalic acid
- TRIALLYL 1,3,5-BENZENETRICARBOXYLATE
- TRI-N-HEXYLTRIMELLITATE