Hexadecyl 3-amino-4-chlorobenzoate Chemical Properties

Boiling point:

495.5±25.0 °C(Predicted)

Density 

1.017±0.06 g/cm3(Predicted)

storage temp. 

under inert gas (nitrogen or Argon) at 2–8 °C

pka

1.48±0.10(Predicted)

CAS DataBase Reference

143269-74-3(CAS DataBase Reference)

EPA Substance Registry System

Benzoic acid, 3-amino-4-chloro-, hexadecyl ester (143269-74-3)

Safety Information

Hazard Codes 

N

Risk Statements 

51/53

Safety Statements 

61

Hexadecyl 3-amino-4-chlorobenzoate Usage And Synthesis

Chemical Properties

White to light brown crystalline powder

Synthesis

A mixture of 16.3 g (0.132 moles) 45percent potassium hydroxide solution, 21.5 g (0.125 moles) of 3-amino-4-chlorobenzoic acid, 100 g of xylene, 40/3 g (0.132 moles) of 1-bromohexadecane and 4.5 g of benzyltriethylammonium bromide (10 mol percent) was heated to reflux. Water was removed using a Dean-Stark trap. After 3 hr at reflux (115-120° C.), the reaction was judged complete by tic. The reaction was cooled to 90° C. and washed with water to remove salts. The solvent was removed on a roto-vap, and the residue was crystallized from heptane to give 40.7 g (83 per cent yield) of a solid Hexadecyl 3-amino-4-chlorobenzoate.

Hexadecyl 3-amino-4-chlorobenzoate(143269-74-3)Related Product Information

• Tris(trimethylsilyl)phosphate
• POLYURETHANE
• 6-Aminocaproic acid
• Glycine
• Dithiooxamide
• Methyl 3-amino-4-chlorobenzoate
• Dodecyl 3-amino-4-chlorobenzoate
• 3-Amino-4-chlorobenzoic acid
• 3-Amino-4-chlorobenzoic acid tetradecyl ester
• N-HEXADECANE-D34
• 3-AMINO-4-CHLOROBENZOIC ACID OCTYL ESTER
• 3-Amino-4-chlorobenzoic acid hexadecyl ester