1,3,5-TRI-N-PROPYL HEXAHYDRO-S-TRIAZINE Chemical Properties

Boiling point:

94℃/0.7mm

Density 

0.880

refractive index 

1.4660

storage temp. 

Sealed in dry,Room Temperature

pka

6.72±0.20(Predicted)

form 

Liquid

color 

Colorless

EPA Substance Registry System

1,3,5-Triazine, hexahydro-1,3,5-tripropyl- (13036-81-2)

Safety Information

TSCA 

Yes

1,3,5-TRI-N-PROPYL HEXAHYDRO-S-TRIAZINE Usage And Synthesis

Synthesis

To a stirred suspension of anhydrous MgSO4 in dichloromethane (25 mL) was sequentially added paraformaldehyde (0.56 g, 18.7 mmol) and freshly distilled n-propylamine (18.7 mmol). The reaction mixture was stirred at room temperature. Upon completion of the reaction, the MgSO4 was removed by filtration and the filtrate was concentrated in vacuum to afford the crude product of 1,3,5-tripropyl-1,3,5-triazacyclohexane, which could be used in the subsequent steps without further purification.

References

[1] Synthesis (Germany), 2018, vol. 50, # 10, p. 2001 - 2008
[2] Journal of the Chemical Society, 1931, p. 1490,1492
[3] Journal of Pharmaceutical Sciences, 1990, vol. 79, # 1, p. 66 - 73
[4] Journal of Polymer Science, Part A: Polymer Chemistry, 2010, vol. 48, # 13, p. 2777 - 2782
[5] Bl.Acad.Belg., vol. <3>26, p. 203;29,30

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