2-Amino-3-chlorobenzoic acid
2-Amino-3-chlorobenzoic acid Basic information
- Product Name:
- 2-Amino-3-chlorobenzoic acid
- Synonyms:
-
- 2-AMINO-3-CHLOROBENZOIC ACID
- BUTTPARK 24\07-98
- 3-CHLORO-2-AMINOBENZOIC ACID
- 3-CHLOROANTHRANILIC ACID
- TIMTEC-BB SBB003844
- 2-Amino-3-chloro
- 2-Amino-3-chlorbenzoesure
- 3-Chloroanthranilic acid (COOH=1)
- CAS:
- 6388-47-2
- MF:
- C7H6ClNO2
- MW:
- 171.58
- EINECS:
- 228-996-4
- Product Categories:
-
- Amines
- Aromatics
- FINE Chemical & INTERMEDIATES
- Phenylacetic acid
- Organic acids
- Miscellaneous Reagents
- benzene derivative
- Aromatic Carboxylic Acids, Amides, Anilides, Anhydrides & Salts
- bc0001
- Mol File:
- 6388-47-2.mol
2-Amino-3-chlorobenzoic acid Chemical Properties
- Melting point:
- 189-191 °C (lit.)
- Boiling point:
- 0°C
- Density
- 1.476±0.06 g/cm3(Predicted)
- Flash point:
- 0°C
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- solubility
- DMSO, Methanaol
- pka
- 4.57±0.10(Predicted)
- form
- Solid
- color
- Yellow to brown
- Water Solubility
- Soluble in water.
- Sensitive
- Air & Light Sensitive
- InChI
- InChI=1S/C7H6ClNO2/c8-5-3-1-2-4(6(5)9)7(10)11/h1-3H,9H2,(H,10,11)
- InChIKey
- LWUAMROXVQLJKA-UHFFFAOYSA-N
- SMILES
- C(O)(=O)C1=CC=CC(Cl)=C1N
- CAS DataBase Reference
- 6388-47-2(CAS DataBase Reference)
Safety Information
- Hazard Codes
- Xi
- Risk Statements
- 36/37/38
- Safety Statements
- 26-37/39-36
- WGK Germany
- 1
- Hazard Note
- Irritant
- HS Code
- 29224999
MSDS
- Language:English Provider:3-Chloroanthranilic acid
- Language:English Provider:ACROS
- Language:English Provider:SigmaAldrich
2-Amino-3-chlorobenzoic acid Usage And Synthesis
Chemical Properties
white to yellow, tan or grey crystalline powder
Uses
2-Amino-3-chlorobenzoic acid is used as pharmaceutical intermediates.
Uses
2-Amino-3-chlorobenzoic Acid is a plant growth regulator.
Synthesis Reference(s)
The Journal of Organic Chemistry, 17, p. 141, 1952 DOI: 10.1021/jo01135a014
Synthesis
The synthesis of 2-Amino-3-chlorobenzoic acid is as follows:
70 ml of methanol was added to an autoclave, and cooled to -70° C., and 16 g (942 mmol) of a generated ammonia gas was added. 30 g (157 mmol) of 2,3-dichlorobenzoic acid and 0.78 g (7.85 mmol) of copper(I) chloride were added. The autoclave was sealed, and heated in an oil bath at 130° C. and 30 atmospheres for 20 hours. After the completion of the reaction, the autoclave was cooled to room temperature, and the reaction mixture was transferred into a reaction flask. 100 ml of water was added to the reaction solution, and the reaction solution was heated in an oil bath to 100° C. to remove the ammonia and the methanol. Then, the reaction solution was cooled to room temperature, and hydrochloric acid was added to adjust the pH value to 3. The precipitated crystals were filtered and dried to obtain 21.8 g of 2-amino-3-chlorobenzoic acid as white crystals with a yield of 81%.
2-Amino-3-chlorobenzoic acid Preparation Products And Raw materials
Preparation Products
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2-Amino-3-chlorobenzoic acid(6388-47-2)Related Product Information
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