ETHYL 2-AMINO-5-METHYLBENZOATE Chemical Properties

Boiling point:

90-92 °C(Press: 0.08 Torr)

Density 

1.103

storage temp. 

under inert gas (nitrogen or Argon) at 2–8 °C

pka

2.52±0.10(Predicted)

Appearance

Yellow to brown Solid

Safety Information

HS Code 

2922498590

ETHYL 2-AMINO-5-METHYLBENZOATE Usage And Synthesis

Synthesis

General procedure for the synthesis of ethyl 2-amino-5-methylbenzoate (compound of formula VII) from 2-amino-5-methylbenzoic acid: following the method reported by SP Acharya and JB Hynes in Journal of Heterocyclic Chemistry (1975,12,1283), the 2-amino-5-methyl benzoic acid was reacted with ethanol catalyzed by HCl gas to obtain the target product. Yield: 80%. The product was a white solid with mass spectrum (ISP) m/z 178 (M-H).

References

[1] Patent: US2003/55042, 2003, A1

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