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N-Acetylethylenediamine

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N-Acetylethylenediamine Basic information

Product Name:
N-Acetylethylenediamine
Synonyms:
  • N-(2-AMINOETHYL)ACETAMIDE
  • N-ACETYLETHYLENEDIAMINE
  • Acetamide, N-(2-aminoethyl-)
  • Acetamide, N-(2-aminoethyl)-
  • N-Monoacetylethylenediamine
  • N-ACETYLETHYLENEDIAMINE, TECH., 90%
  • 2-(acetamido)ethylamine
  • N-AcetylethylenediaMine , 95.0%(GC)
CAS:
1001-53-2
MF:
C4H10N2O
MW:
102.14
Product Categories:
  • Intermediates of Dyes and Pigments
Mol File:
1001-53-2.mol
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N-Acetylethylenediamine Chemical Properties

Melting point:
50 °C (lit.)
Boiling point:
128 °C/3 mmHg (lit.)
Density 
1.066 g/mL at 25 °C (lit.)
refractive index 
n20/D 1.485(lit.)
Flash point:
>230 °F
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
solubility 
DMSO (Slightly), Methanol (Slightly)
form 
Solid
pka
15.97±0.46(Predicted)
color 
White to Yellow Low-Melting
Sensitive 
Hygroscopic
BRN 
1743120
CAS DataBase Reference
1001-53-2(CAS DataBase Reference)
NIST Chemistry Reference
N-Acetylethylenediamine(1001-53-2)
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Safety Information

Risk Statements 
34
Safety Statements 
23-24/25-36/37/39-26
RIDADR 
3259
WGK Germany 
3
3
HazardClass 
8
PackingGroup 
III
HS Code 
29241990

MSDS

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N-Acetylethylenediamine Usage And Synthesis

Chemical Properties

White to yellow crystalline solid

Uses

N-(2-Aminoethyl)acetamide may be used in the preparation of mixed two-component monolayers on glassy carbon. It may be used in the synthesis of lysidine.

General Description

N-(2-Aminoethyl)acetamide is an organic building block.

Purification Methods

The acetyl-diamine has been fractionated under reduced pressure and fraction b 125-130o/5mm was refractionated, fraction b 132-135o/4mm was collected and solidified. It is a low melting hygroscopic solid which can be recrystallised from dioxane/Et2O. It is soluble in H2O, Et2O and *C6H6. The p-toluenesulfonate salt can be recrystallised from EtOH/EtOAc (1:8), has m 125-126o but the free base cannot be recovered from it by basifying and extracting with CH2Cl2. The picrate has m 175o (from EtOH) [Aspinall J Am Chem Soc 63 853 1941, Hall J Am Chem Soc 78 2570 1956]. [Beilstein 4 IV 1193.]

N-Acetylethylenediamine Preparation Products And Raw materials

Raw materials

N-AcetylethylenediamineSupplier

Creasyn Finechem(Tianjin) Co., Ltd.
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