3-Iodo-9H-carbazole Chemical Properties

Melting point:

195-197℃

Boiling point:

430.6±18.0 °C(Predicted)

Density 

1.854

storage temp. 

Keep in dark place,Sealed in dry,Room Temperature

form 

powder to crystal

pka

16.54±0.30(Predicted)

color 

White to Light yellow to Light orange

λmax

340nm(CH3CN)(lit.)

InChI

InChI=1S/C12H8IN/c13-8-5-6-12-10(7-8)9-3-1-2-4-11(9)14-12/h1-7,14H

InChIKey

OYIGWMXXIFYAGD-UHFFFAOYSA-N

SMILES

N1C2=C(C=CC=C2)C2=C1C=CC(I)=C2

Safety Information

HS Code 

2933.99.8290

3-Iodo-9H-carbazole Usage And Synthesis

Description

3-Iodo-9H-carbazole is a chemical compound used in the research and development of organic materials for optoelectronic devices, such as OLEDs (organic light-emitting diodes). It has also been studied for its potential use in pharmaceuticals. It may cause skin and eye irritation, respiratory issues, and other health hazards if not handled properly. Therefore, it must be stored in a well-ventilated area, away from heat sources or combustible materials.

Synthesis

A solution of 9H-carbazole (5.57g, 33.3 mmol) and KI (3.68g, 22.2 mmol) in AcOH (92 mL) was heated to 100 °C for 1 h. KI03 (3.57g, 16.7 mmol) was added in portions to the solution, and the resulting mixture was stirred for another 2 h at 100°C. The mixture was poured into water (500 mL), and the precipitation was collected by filtration and washed with hot water. Recrystallization was made in DCM to afford 6.8 g (70 percent) of product 3-Iodo-9H-carbazole as a white solid.

3-Iodo-9H-carbazole(16807-13-9)Related Product Information

• 2-chloro-9H-carbazole
• 4-BroMo-9H-carbazole
• 3-Bromo-9H-carbazole
• 2-phenyl-9H-carbazole
• 3-phenyl-9H-carbazole
• 2-BROMOCARBAZOLE