1,3-Dichloro-2,2-dimethoxypropane Chemical Properties

Melting point:

81.5 °C

Boiling point:

194.0±35.0 °C(Predicted)

Density 

1.180±0.06 g/cm3(Predicted)

storage temp. 

Sealed in dry,Room Temperature

Appearance

White to off-white Solid

Safety Information

HS Code 

2909199090

1,3-Dichloro-2,2-dimethoxypropane Usage And Synthesis

Synthesis

In a 150 mL three-neck flask, 17.42 g of acetone and 43.55 g of methanol were added, the reaction temperature was controlled in the range of 20-35 °C, and chlorine gas was slowly passed through. When the chlorine gas was passed in an amount of about 42.0 g, the chlorine gas was stopped and the reaction mixture was continued to be stirred for 0.5 hours. Subsequently, the reaction mixture was cooled to 0-5 °C, and filtration was carried out to afford 42.24 g of 1,3-dichloro-2,2-dimethoxypropane in 81.2% yield.

References

[1] Patent: CN105461529, 2016, A. Location in patent: Paragraph 0012; 0020

1,3-Dichloro-2,2-dimethoxypropane(6626-57-9)Related Product Information

• METHYL N-PROPYL ETHER
• N,N-Dimethylacetamide
• 1-Bromopropane
• Propane
• 2,2-Dimethoxypropane
• 1,1-Dimethoxyethane
• Diphenyldimethoxysilane
• Dimethyldimethoxysilane
• 1,2,3,4-Tetrachloro-5,5-dimethoxycyclopentadiene
• 2,3,5,6-TETRACHLORO-4,4-DIMETHOXYPENTACYCLO[5.4.0.0(2,6).0(3,10).0(5,9)]UNDECANE-8,11-DIONE
• 1,9,10,11-TETRACHLORO-12,12-DIMETHOXY-5-OXATETRACYCLO[7.2.1.0(2,8).0(4,6)]DODEC-10-ENE-3,7-DIONE
• DIMETHOXYPROPANE
• 1,8,9,10-TETRACHLORO-11,11-DIMETHOXYTRICYCLO[6.2.1.0(2,7)]UNDECA-4,9-DIENE-3,6-DIONE
• 1,9,10,11-TETRACHLORO-12,12-DIMETHOXY-4-METHYL-5-OXATETRACYCLO[7.2.1.0(2,8).0(4,6)]DODEC-10-ENE-3,7-DIONE
• 1,8,9,10-TETRACHLORO-11,11-DIMETHOXY-4-METHYLTRICYCLO[6.2.1.0(2,7)]UNDECA-4,9-DIENE-3,6-DIONE
• 1,3-Dichloro-2,2-dimethoxypropane