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Caulophylline

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Caulophylline Basic information

Product Name:
Caulophylline
Synonyms:
  • N-METHYLCYTISINE
  • (1r)-l
  • 1,5-methano-8h-pyrido(1,2a)(1,5)diazocin-8-one,1,2,3,4,5,6-hexahydro-3-methy
  • 1,5-Methano-8H-pyrido[1,2-a][1,5]diazocin-8-one, 1,2,3,4,5,6-hexahydro-3-methyl-, (1R)-
  • 1,5-Methano-8H-pyrido[1,2-a][1,5]diazocin-8-one, 1,2,3,4,5,6-hexahydro-3-methyl-, (1R-cis)-
  • 12-methyl-cytisin
  • 12-Methylcytisine
  • Caulophyllin
CAS:
486-86-2
MF:
C12H16N2O
MW:
204.27
EINECS:
207-643-8
Product Categories:
  • chemical reagent
  • pharmaceutical intermediate
  • Miscellaneous Reagents
  • phytochemical
  • reference standards from Chinese medicinal herbs (TCM).
  • standardized herbal extract
Mol File:
486-86-2.mol
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Caulophylline Chemical Properties

Melting point:
137-139oC
alpha 
30D -224° (c = 1.05 in water)
Boiling point:
342.77°C (rough estimate)
Density 
1.0565 (rough estimate)
refractive index 
1.6000 (estimate)
storage temp. 
-20°C Freezer, Under Inert Atmosphere
solubility 
Chloroform (Slightly), Ethyl Acetate (Slightly), Methanol (Slightly)
form 
powder
pka
9.61±0.20(Predicted)
color 
White to Off-White
NIST Chemistry Reference
Caulophylline(486-86-2)
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Safety Information

Hazard Codes 
Xn
Risk Statements 
22
WGK Germany 
3
RTECS 
HA4400000
Toxicity
LD50 in mice (mg/kg): 21 i.v.; 51 i.p. (Barlow, McLeod)
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Caulophylline Usage And Synthesis

Description

This base was first prepared synthetically by Partheil and subsequently discovered in the roots of Caulophyllurn thalictroides L. It is widespread among the Papilionaceae, being found in Baptisia australis, Genista tinctoria, Sophora microphylla, S. tetraptera, Thermopsis lanceolata and T. rhombifolia (Watt.) Richards. It is laevorotatory with [α]20D - 221 ° (H20) and furnishes the following crystalline salts and derivatives: hydrochloride, m.p. 2S0-SoC (dec.); hydriodide, m.p. 246-7°C (dec.); perchlorate, m.p. 2S4°C (dec.); aurichloride, m.p. 206°C (dec.); picrate, m.p. 230°C; picrolonate, m.p. 224-SoC (dec.) and the methiodide which occurs in two modifications, m.p. 248°C and 267-276°C.

Chemical Properties

Colourless Needles

Uses

N-Methylcytisine (cas# 486-86-2) is a compound useful in organic synthesis.

General Description

N-Methylcytisine is a nicotinic alkaloid found in Caulophyllum thalictroides, also known as blue cohosh.

Hazard

Extremely toxic; cardiotoxic; poisonous.

Biochem/physiol Actions

N-Methylcytisine is toxic and binds selectively to nicotinic acetylcholine receptors in the CNS.

References

Partheil., Arch. Pharm., 230,448 (1892)
Power, Salway., J. Chem. Soc., 103, 194 (1913)

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