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Tris(acetonitrile)tricarbonyltungsten

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Tris(acetonitrile)tricarbonyltungsten Basic information

Product Name:
Tris(acetonitrile)tricarbonyltungsten
Synonyms:
  • tris(acetonitrile)tricarbonyl-tungste
  • TRIS(ACETONITRILE)TRICARBONYLTUNGESTEN(&
  • tris(acetonitrile)tricarbonyltungsten(0)
  • tris(acetonitrile)tungsten(0)
  • Tris(acetonitryl)tungsten tricarbonyl
  • Tricarbonyl tris(acetonitrile)tungsten
  • Tris(acetonitrile)tungsten tricarbonyl
  • TRIS(ACETONITRILE)TRICARBONYLTUNGSTEN
CAS:
16800-47-8
MF:
C9H9N3O3W
MW:
391.03
EINECS:
240-833-9
Mol File:
16800-47-8.mol
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Tris(acetonitrile)tricarbonyltungsten Chemical Properties

Melting point:
>300 °C(lit.)
Boiling point:
34°C
solubility 
sol acetonitrile, nitromethane
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Safety Information

Hazard Codes 
T+
Risk Statements 
26/27/28
Safety Statements 
28-36/37-45-7/9
RIDADR 
UN 3466 6.1/PG 1
WGK Germany 
3
RTECS 
YO7800000
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Tris(acetonitrile)tricarbonyltungsten Usage And Synthesis

Uses

Catalyst for allylic substitutions

Reactant for:

  • Mixed disilyl-substituted cyclopentadiene derivatives
  • Synthesis of catalytically active ansa compounds with cycloalkyl moieties
  • Stepwise assembly of mixed metal dinuclear carbonyl complexes
  • Cycloaddition of M(CO)3-coordinated-cyanoazepine with alkynes

Preparation

By refluxing Hexacarbonyltungsten in Acetonitrile in an inert atmosphere. Removal of solvent under an  inert atmosphere yields tris(acetonitrile)tricarbonyltungsten. Solutions of the reagent can be prepared by photolysis of  hexacarbonyltungsten in acetonitrile.

reaction suitability

core: tungsten
reagent type: catalyst

storage

Air and thermally sensitive; pyrophoric. Use in a fume hood.

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