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Dicyclohexano-18-crown-6

Basic information Safety Supplier Related

Dicyclohexano-18-crown-6 Basic information

Product Name:
Dicyclohexano-18-crown-6
Synonyms:
  • cis-Dicyclohexano-18-crown-6, cis-syn-cis isomer, 98+%
  • cis-Dicyclohexano-18-crown-6, mixture of syn-cis and anti-cis isomers, 98%
  • d2-06
  • Dibenzo[b,k][1,4,7,10,13,16]hexaoxacyclooctadecin, eicosahydro-
  • Dicyclohexo-18-crown-6
  • Eicosahydro-5,8,11,16,19,22-hexaoxadibenzo[a,j]cyclooctadecene
  • Icosahydrodibenzo[b,k][1,4,7,10,13,16]hexaoxacyclooctadecine
  • k)(1,4,7,10,13,16)hexaoxacyclooctadecin,eicosahydro-dibenzo(
CAS:
16069-36-6
MF:
C20H36O6
MW:
372.5
EINECS:
240-216-4
Product Categories:
  • Crown Ethers
  • Functional Materials
  • Macrocycles for Host-Guest Chemistry
Mol File:
16069-36-6.mol
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Dicyclohexano-18-crown-6 Chemical Properties

Melting point:
47-50 °C
Boiling point:
344°C
Density 
1.102 g/cm
refractive index 
1.4909
Flash point:
113 °C
storage temp. 
Store below +30°C.
form 
Crystalline Solid
color 
White to slightly beige
Water Solubility 
Slightly soluble
Sensitive 
Hygroscopic
Merck 
14,2602
BRN 
1130529
CAS DataBase Reference
16069-36-6(CAS DataBase Reference)
NIST Chemistry Reference
Dicyclohexano-18-crown-6(16069-36-6)
EPA Substance Registry System
Dibenzo[b,k][1,4,7,10,13,16]hexaoxacyclooctadecin, eicosahydro- (16069-36-6)
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Safety Information

Hazard Codes 
T,Xn
Risk Statements 
23/24/25-36/37/38-20/21/22-36/38-22
Safety Statements 
26-36/37/39-45-38-28A-36
RIDADR 
UN 2811 6.1/PG 3
WGK Germany 
3
RTECS 
HP5385000
3-9
TSCA 
Yes
HazardClass 
6.1
PackingGroup 
III
HS Code 
29329995
Toxicity
LD50 orally in Rabbit: 176 mg/kg

MSDS

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Dicyclohexano-18-crown-6 Usage And Synthesis

Chemical Properties

White solid

Uses

Dicyclohexano is used as an anion activator and complexing agent which solubilizes alkali metal ions in non-polar solvents. It is an important raw material and intermediate used in Organic Synthesis, Pharmaceuticals, Agrochemicals and Dyestuffs etc,.

Uses

Anion activator, and complexing agent which solubilizes alkali metal ions in non-polar solvents.

Safety Profile

Poison by ingestion, skin contact, and intraperitoneal routes. An experimental teratogen. An eye and skin irritant. When heated to decomposition it emits acrid smoke and fumes.

Purification Methods

Purify it by chromatography on neutral alumina and eluting with an ether/hexane mixture [see Izatt et al. Inorg Chem 14 3132 1975]. Dissolve it in ether at ca 40o, and spectroscopic grade MeCN is added to the solution, which is then chilled. The crown ether precipitates and is filtered off. It is dried in vacuo at room temperature [Wallace J Phys Chem 89 1357 1985]. [V.gtle ed. Top Corr Chem (Host Guest Complex Chemistry) 98 1981.] SKIN IRRITANT.

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