N,N-DIMETHYL-4,4'-AZODIANILINE
N,N-DIMETHYL-4,4'-AZODIANILINE Basic information
- Product Name:
- N,N-DIMETHYL-4,4'-AZODIANILINE
- Synonyms:
-
- 4-((4-aminophenyl)azo)-n,n-dimethyl-benzenamin
- 4-((4-aminophenyl)azo)-n,n-dimethylbenzenamine
- 4-(p-dimethylaminophenylazo)-anilin
- 4-[(4-aminophenyl)azo]-n,n-dimethyl-benzenamin
- c.i.disperseblack3
- Diazo nero microsetile G
- diazoneromicrosetileg
- Interchem acetate developed black
- CAS:
- 539-17-3
- MF:
- C14H16N4
- MW:
- 240.3
- EINECS:
- 208-712-5
- Mol File:
- 539-17-3.mol
N,N-DIMETHYL-4,4'-AZODIANILINE Chemical Properties
- Melting point:
- 190-195 °C (dec.)
- Boiling point:
- 373.02°C (rough estimate)
- Density
- 1.0236 (rough estimate)
- refractive index
- 1.4850 (estimate)
- storage temp.
- 2-8°C
- form
- powder to crystal
- pka
- 3.43±0.10(Predicted)
- color
- Yellow to Amber to Dark red
- Water Solubility
- 120.2ug/L(25 ºC)
- BRN
- 748253
- InChIKey
- BVRIUXYMUSKBHG-WUKNDPDISA-N
- CAS DataBase Reference
- 539-17-3(CAS DataBase Reference)
- EPA Substance Registry System
- Benzenamine, 4-[(4-aminophenyl)azo]-N,N-dimethyl- (539-17-3)
MSDS
- Language:English Provider:SigmaAldrich
- Language:English Provider:ACROS
N,N-DIMETHYL-4,4'-AZODIANILINE Usage And Synthesis
Chemical Properties
dark orange to rust brown crystalline powder
Uses
N,?N-?Dimethyl-?4,?4''-?azodianiline is a disperse dye. Dyes and metabolites.
Preparation
4-Nitrobenzenamine diazo, and N,N-dimethylaniline?coupling, and then will the nitro reductive into amino.
Safety Profile
Poison by intraperitoneal route. Mutation data reported. When heated to decomposition it emits toxic fumes of NOx
Properties and Applications
black, red and black. Red crystallization, melting point of 186 ~ 187 ℃. Soluble in ethanol, acetone, soluble fiber element, pottery, solvent and carbon tetrachloride,. The strong sulfuric acid is palm in light yellow, diluted for orange red; In the light of nitric acid for palm red solution; In strong hydrochloric acid solution for red; In the thick of sodium hydroxide solution don’t change color.
| Standard(Polyamide) | Ironing Fastness | Light Fastness | Persperation Fastness | Washing Fastness | |||
| Fading | Stain | Fading | Stain | Fading | Stain | ||
| ISO | 2 | 3 | 4 | 3-4 | 4 | 4 | |
Purification Methods
Crystallise the azo-dye from aqueous EtOH. [Beilstein 14 IV 1004.]
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N,N-DIMETHYL-4,4'-AZODIANILINE(539-17-3)Related Product Information
- Disperse Blue 79
- DISPERSE RED 19
- Disperse Orange 25
- Disperse Red 5
- DISPERSE RED 13
- DISPERSE RED 17
- Disperse Blue 183
- 2-[N-(2-Cyanoethyl)-4-[(2,6-dichloro-4-nitrophenyl)azo]anilino]ethyl acetate
- N,N-DIMETHYL-4,4'-AZODIANILINE
- 4-(N,N-DIMETHYLAMINO)AZOBENZENE-4'-ISOTHIOCYANATE
- Disperse Violet 33
- Disperse Red 73
- 4'-NITRO-4-DIMETHYLAMINOAZOBENZENE
- DISPERSE BLACK 9
- Disperse Red 1
- Disperse Brown 1
- 4,4'-AZODIANILINE
- Azobenzene