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4-Bromo-N,N-dimethylaniline

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4-Bromo-N,N-dimethylaniline Basic information

Product Name:
4-Bromo-N,N-dimethylaniline
Synonyms:
  • P-BROMO-N,N-DIMETHYLANILINE
  • N,N-DIMETHYL-P-BROMOANILINE
  • N-(4-BROMOPHENYL)-N,N-DIMETHYLAMINE
  • (4-Bromo-phenyl)-dimethyl-amine
  • 1-Bromo-4-(dimethylamino)benzene
  • 4-(Dimethylamino)phenyl bromide
  • 4-(dimethylamino)phenylbromide
  • 4-bromo-dimethylaniline
CAS:
586-77-6
MF:
C8H10BrN
MW:
200.08
EINECS:
209-582-2
Product Categories:
  • Miscellaneous
  • Building Blocks
  • Anilines, Aromatic Amines and Nitro Compounds
  • Chemical Synthesis
  • Nitrogen Compounds
  • Organic Building Blocks
  • Aniline
  • Amines
  • C8
  • Nitrogen Compounds
  • bc0001
  • 586-77-6
Mol File:
586-77-6.mol
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4-Bromo-N,N-dimethylaniline Chemical Properties

Melting point:
52-54 °C (lit.)
Boiling point:
264 °C (lit.)
Density 
1.3220
refractive index 
1.5748 (estimate)
Flash point:
>230 °F
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
solubility 
Chloroform, Methanol
form 
Crystalline Solid
pka
4.23(at 25℃)
color 
White to gray or light blue
Water Solubility 
Soluble in methanol. Insoluble in water.
BRN 
2206155
Stability:
Stable. Incompatible with oxidizing agents, acids, metals.
InChIKey
XYZWMVYYUIMRIZ-UHFFFAOYSA-N
CAS DataBase Reference
586-77-6(CAS DataBase Reference)
NIST Chemistry Reference
4-Bromo-N,N-dimethylaniline(586-77-6)
EPA Substance Registry System
N,N-Dimethyl-p-bromoaniline (586-77-6)
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Safety Information

Hazard Codes 
Xn,Xi
Risk Statements 
20/21/22-36/38-33-22
Safety Statements 
26-36-45-37-28A
RIDADR 
2811
WGK Germany 
3
RTECS 
BW9300000
8
Hazard Note 
Irritant
TSCA 
Yes
HazardClass 
6.1(b)
PackingGroup 
III
HS Code 
29214290

MSDS

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4-Bromo-N,N-dimethylaniline Usage And Synthesis

Chemical Properties

white to light grey powder

Uses

4-Bromo-N,N-dimethylaniline is used as an internal standard in the determination of iodine present as iodide (as in pharmaceuticals), iodate (as in iodized table salt) and covalently bound to organic compounds (as in milk and vegetables).

Purification Methods

Reflux the aniline for 3hours with two equivalents of acetic anhydride, then fractionally distil it under reduced pressure. [Beilstein 12 IV 1499.]

4-Bromo-N,N-dimethylaniline Preparation Products And Raw materials

Preparation Products

Raw materials

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